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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone: (209) 384-2930 <br /> Certificate #2480 Fax: (209) 384-1507 <br /> Technicon Engineering Client Project Name: 180321 Method: EPA 5030/62608 <br /> 4539 N. Brawley #108 Lab Reference Number: 1910022 Instrument ID: VARIAN MS <br /> Fresno, CA 93722 Sample Description: Soil Prepared: 10-10-19 <br /> Attn: Steve Curra Analyzed: 10-10-19 <br /> Reported: 10-16-19 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VSMS-0109 DP <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kg mg/K -mg/Kg %R <br /> COMPOUNDS <br /> t-But Alcohol t-BA) 0. 10 NO 3.0 100% 70-130 <br /> Meth I t-but ether MTBE) 0.0050 NO 0. 10 104% 70-130 <br /> Diisopra lether DIPE 0.0050 ND 0. 10 94.4% 70-130 <br /> Eth II I ether (ETBE 0.0050 ND 0. 10 88.8% 70-130 <br /> t-Am meth I ether TAME 0.0050 ND 0. 10 84.8% 70-130 <br /> 1 ,2-Dichloroethane 1 ,2-DCA 0.0050 NO 0. 10 85.6% 70-130 <br /> Ethylene dibromide EDB 0.0050 ND 0. 10 110% 70-130 <br /> 111 -Dichloroethene It , 1 Dui:'2 0.0050 ND 0. 10 102% 70-130 <br /> Benzene 0.0050 NO 0. 10 90.0% 70-130 <br /> Trichloroethene (TCE) 0.0050 ND 0. 10 85.6% 70-130 <br /> Toluene 0.0050 ND 0. 10 87.2% 70- 130 <br /> Chlorobenzene 0.0050 ND 0. 10 94.0% 70-130 <br /> Surro ate: <br /> Dibromofluoromethane 0. 10 95. 3% 0.40 94.5% 70-130 <br /> 1 ,2-Dichloroethane-d4 0. 10 89.6% 0.40 101 % 70-130 <br /> Toluene-dB 0. 10 98.8% 0.40 104% 70-130 <br /> 4-Bromofluorobenzene 0. 10 115% 0.40 119% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> mg/Kg %R %R <br /> COMPOUNDS <br /> t-Butyl Alcohol t-BA 3.0 70.2% 73.7% 60-130% 4,86% <br /> Methyl t-but I ether MTBE 0. 10 87.6 % 93.6 % 70-130% 6.62 <br /> Diiso ro I ether DIPE 0. 10 75.6% 75.6% 70-130% 0.00 <br /> Eth I t-But I ether (ET E) 0. 10 78.8% 79.2% 70-130% 0.51 % <br /> t-Am I meth I ether (TAME) 0. 10 70.8% 77.2% 70-130% 8. 120o <br /> 1 ,2-Dichloroethane 112-DCA 0. 10 77.2% 83.6% 70-130% 7.96% <br /> Eth lenedibromide EDB) 0. 10 97.2% 106% 70-130% 9.04% <br /> 1 , 1 -Dichloroethene 1 , 1 , D(;E) 0. 10 93.2% 99.2% 60-130% 6.24% <br /> Benzene 0. 10 79.6% 82.8% 70-130% 3.77% <br /> Trichloroethene TCE 0. 10 92 .8% 93.6% 70-130% 0.86% <br /> Toluene 0. 10 7942% 88.0% 70-130% 9.95% <br /> Chlorobenzene 0. 10 90.00/0 90.4% 70-130% 0443% <br /> Surrogate: <br /> Dibromofluoromethane 0.40 92.8% 92.8% 70-130% 0.00% <br /> 1 ,2-Dichloroethane-d4 0.40 93. 0% 100% 70-130% 7.35% <br /> Toluene-d8 0.40 101 % 104% 70-130% 2.84% <br /> 4-Bromofluorobenzene 0.40 16% 116% 70-130% 0.09% <br /> APPROVED BY: <br /> Clari J. Cone / Lab ratory irector <br /> Cassandra J.A. N nney / Chemist <br />