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tri i <br />819 Striker Avenue. Suite 8 <br />Sacramento.. CA 95834 <br />(916; 921-9600 <br />FAX (916) 92 1 -0100 <br />www.sequoialaos.com <br />Kleinfelder - Stockton Project: Granite Burnpile <br />2825 East Myrtle Street Project Number: 20-1108-33 Reported: <br />Stockton CA. 95205 Project Manager: Doug Heard 08/15/01 17:2.1 <br />Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br />Sequoia Analytical - Walnut Creek <br />Reporting Spike Source %REC RPD <br />malvte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch 1H02022 - EPA 3550B Sonication <br />Blank (1H02022-BLKl) <br />Prepared: 08/02/01 Analyzed: 08/04/01 <br />2,4-Dinitrotoluene <br />ND <br />0.20 <br />mg/kg <br />2,6-Dinitrotoluene <br />ND <br />0.20 <br />" <br />Di-n-octyl phthalate <br />ND <br />0.20 <br />" <br />Fluoranthene <br />ND <br />0.10 <br />- <br />Fluorene <br />ND <br />0.10 <br />" <br />Hexachlorobenzene <br />ND <br />0.20 <br />" <br />Hexachlorobutadiene <br />ND <br />0.20 <br />" <br />Hexachlorocyclopentadiene <br />ND <br />0.20 <br />" <br />Hexachloroethane <br />ND <br />0.20 <br />" <br />Indeno (1,2,3 -cd) pyrene <br />ND <br />0.10 <br />" <br />Isophorone <br />ND <br />0.20 <br />" <br />2 -Methylnaphthalene <br />ND <br />0.20 <br />" <br />2-Methylphenol <br />ND <br />0.10 <br />" <br />4-Methylphenol <br />ND <br />0.10 <br />" <br />Naphthalene <br />ND <br />0.10 <br />" <br />2-Nitroaniline <br />ND <br />0.50 <br />" <br />3-Nitroaniline <br />ND <br />0.50 <br />" <br />4-Nitroaniline <br />ND <br />0.50 <br />" <br />Nitrobenzene <br />ND <br />0.20 <br />" <br />2-Nitrophenol <br />ND <br />0.10 <br />" <br />N-Nitrosodimethylamine <br />ND <br />0.10 <br />" <br />4-Nitrophenol <br />ND <br />0.50 <br />" <br />N-Nitrosodiphenylamine <br />ND <br />0.20 <br />N-Nitrosodi-n-propylamine <br />ND <br />0.10 <br />" <br />Pentachlorophenol <br />ND <br />0.50 <br />" <br />Phenanthrene <br />ND <br />0.10 <br />" <br />Phenol <br />ND <br />0.10 <br />" <br />Pyrene <br />ND <br />0.20 <br />, <br />1,2,4-Trichlorobenzene <br />ND <br />0.20 <br />, <br />2,4,5 -Trichlorophenol <br />ND <br />0.10 <br />" <br />2.4,6 -Trichlorophenol <br />ND <br />0.10 <br />" <br />Surrogate: 2-Fluorophenol <br />3.69 <br />5.00 <br />73.8 25-121 <br />Surrogate: Phenol -d6 <br />3.82 <br />5.00 <br />76.4 24-113 <br />Surrogate: Nurobenzene-d5 <br />2.37 <br />3.33 <br />711 23-120 <br />Surrogate: _'-Fluorobiphenyl <br />2.92 <br />3.33 <br />87.7 30-115 <br />Sequoia Analytical - Sacramento The resulls in this report apply, to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirely. <br />Paae 16 of 20 <br />