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® 819 Striker Avenue, Suite 8 <br />Seq <br />Sacramento, CA 95834 <br />(916) 921-9600 <br />FAX (916) 921 -0 100 <br />Analytical <br />www.sequoialabs.com <br />Kleinfelder - Stockton Project: Granite Bumpile <br />2825 East Myrtle Street Project Number: 20-1108-33 Reported: <br />Stockton CA, 95205 Project Manager: Doug Heard 08/15/01 1-:24 <br />Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br />Sequoia Analytical - Walnut Creek <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch 1HO2022 - EPA 3550B Sonication <br />Matrix Spike Dup (1H02022-MSDl) <br />Source: W107390-01 <br />Prepared: 08/02/01 Analyzed: 08/04/01 <br />Surrogate: Nitrobe=ene-d5 <br />2.46 mg/kg <br />3.33 <br />73.9 <br />23-120 <br />Surrogate:2-Fluorobiphenyl <br />2.99 <br />3.33 <br />89.8 <br />30-115 <br />Surrogate: 2,4,6-Tribromophenol <br />3.11 <br />5.00 <br />62.2 <br />19-122 <br />Surrogate: p-Terphenyl-d/4 <br />3.61 <br />- 3.33 <br />108 <br />18-137 <br />Sequoia Analytical - Sacramento The results in this report apply to the samples anal;y:.ed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its enuren,. <br />Page 19 of 20 <br />v <br />