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4 4 Sequoia <br />wo <br />Analytical ,,,' <br />m <br />819 Striker Avenue, Suite 8 <br />1610 Sacramento, CA 95834 <br />(916) 921-9600 <br />FAX (916) 921-0100 <br />www.sequoialabs.com <br />Kleinfelder - Stockton Project: Granite Burnpile <br />2825 East Myrtle Street Project Number: 20-1108-33 Reported: <br />Stockton CA, 95205 Project Manager: Doug Heard 08/15/01 17:24 <br />Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br />Sequoia Analytical - Walnut Creek <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Ratch 1H02022 -EPA 3550B Sonication <br />Matrix Spike Dup (1H02022-MSD1) <br />Source: W107390-01 Prepared: 08/02/01 Analyzed: 08/04/01 <br />- <br />Surrogate: Nitrobenzene -d5 --_- - <br />2.46 -mg/kg 3.33 73.9 23-120 <br />Surrogate:2-Fluorobiphenyl <br />2.99 3.33 89.8 30-115 <br />Surrogate: 2,4,6-Tribromophenol <br />3.11 5.00 62.2 19-122 <br />Surrogate: p-Terphenyl-d14 <br />3.61 3.33 108 18-137 <br />Sequoia Analytical - Sacramento The results in this report apply to the samples analyzed in accordance with the chain of <br />custody document. This analytical report must be reproduced in its entirety. <br />Page 19 of 20 <br />