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THE REPORT DATE : January 2, 2003 THE TWINING LABORATORIES, INC <br /> T WINING LABORATORY ID 702-6348.5 PAGE 4 of z <br /> DATE SAMPLED : 12/11/02 at 0930 by Brian Bock UNIT: ug/L <br /> DATE RECEIVED : 12/12/02 at 1315 from Eddie Walters METHOD: EPA 62E <br /> DATE PREPARED 12/30/02 DATE ANALYZED: 12/30/02 <br /> ANALYZED BY C. Fammatre REVIEWED BY: C. FammatrE <br /> L A B 0 R A T 0 R I E S I N C CLIENT SAMPLE ID Lodi Chrome SAMPLE TYPE: Waste Watel <br /> F- CONSTITUENT RESULT DLR CONSTITUENT RESULT DLR <br /> Acenaphthene ND 10 1,2-Dichlorobenzene ND 10 N-Nitrosodiphenylamine ND 10 <br /> Acenaphthylene ND 10 3,3'-Dichlorobenzidine ND 10 N-Nitrosodi-n-propylamine ND 10 <br /> Anthracene ND 10 2,4-Dichlorophenol ND 10 Pentachlorophenol ND 10 <br /> Benzidine ND 10 Diethylphthalate ND 10 Phenanthrene ND 10 <br /> Benzo(a)anthracene ND 10 Dimethylphthalate ND 10 Phenol ND 10 <br /> Benzo(a)pyrene ND 10 2,4-Dimethylphenol ND 10 Pyrene ND 10 <br /> Benzo(b)fluoranthene ND 10 2,4-Dinitrophenol ND 10 1,2,4-Tirchlorobenzene ND 10 <br /> Benzo(g,h,i) perylene ND 10 2,4-Dinitrotoluene ND 10 2,4,6-Trichlorophenol ND 10 <br /> Benzo (k)fluoranthene ND 10 2,6-Dinitrotoluene ND 10 Aldrin ND 10 <br /> Bis(2-chloroethoxy)methane ND 10 Di-n-octylphth a late ND 10 b-BHC ND 10 <br /> Bis(2-chloroethyl)ether ND 10 Fluoranthene ND 10 d-BHC ND 10 <br /> Bis(2-chloroisopropyl)ether ND 10 Fluorene ND 10 4,4'-DDD ND 10 <br /> Bis(2-ethylhexyl)phthalate ND 10 Hexachlorobenzene ND 10 4,4'-DDE ND 10 <br /> 4-Bromophenyl phenyl ether ND 10 Hexachlorobutadiene ND 10 4,4'-DDT ND 10 <br /> Butyl benzyl phthalate ND 10 Hexachlorocyclopentadiene ND 10 Dieldrin ND 10 <br /> 2-Chloronaphthalene ND 10 Hexachloroethane ND 10 Endosulfan Sulfate ND 10 <br /> 4-Chloro-3-methyl phenol ND 10 Indeno(1,2,3-cd)Pyrene ND 10 Endrin Aldehyde ND 10 <br /> 2-Chlorophenol ND 10 Isophorone ND 10 Heptachlor ND 10 <br /> 4-Chlorophenyl phenyl ether ND 10 2-Methyl-4,6-dinitrophenol ND 10 Heptachlor epoxide ND 10 <br /> Chrysene ND 10 Naphthalene ND 10 SURROGATE RECOVERY RANGE <br /> Dibenzo(a,h)Anthracene ND 10 Nitrobenzene ND 10 2-Fluorophenol 26.2 21-100% <br /> Di-n-butylphthalate ND 10 2-Nitrophenol ND 10 Phenol-D6 47.3 10-94% <br /> 1,3-Dichlorobenzene ND 10 4-Nitrophenol ND 10 Nitrobenzene-D-5 36.8 35-114% <br /> x <br /> 1,4-Dichlorobenzene ND 10 N-Nitrosodimethylamine ND 10 2-Fluorobiphenyl 46.4 43-116% <br /> 2,4,6-Tribromophenol 94.2 10-123% <br /> D14-Terphenyl 80.0 70-130% <br /> ug/L,micrograms per Liter(parts per billion) ND.None Detected DLR.Detection Limit for Reporting purposes <br /> Rev. 2 12/02(625) <br />