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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> M c C a m p b e I l Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When Quality Counts" I <br /> http://www.mccampbeR.com/E-mail:main@mccampbell.com <br /> California Department of Fish and Wildlife Client Project ID: Solid Wet Waste Date Sampled: 02/11/16 <br /> Date Received: 02/12/16 <br /> Bay Delta,Region 3 <br /> 2109 Arch Airport Road,Suite Client Contact: Kathy Hieb Date Extracted: 02/16/16-02/20/16 <br /> Stockton,CA 95206 Client P.O.: Date Analyzed: 02/16/16-02/20/16 <br /> CA Title 22 Acute Fish Bioassay Screen Test for Hazardous Waste <br /> Extraction Method: CA DFG(Polisim&Miller) Analytical Method: CA DFG(Polisini&Miller) Work Order: 1602408 <br /> Lab ID 1602408-002A Species Pimephales promelas Avg.Length(mm) 36.12 <br /> Client ID Composite#2 Common Name Fathead Minnows Avg.Weight(g) 0.349 <br /> Matrix Solid Max Weight(g) 0.398 <br /> Control Water Soft Synthetic Water Min Weight(g) 0.266 <br /> Survival Dissolved 02(mg/L) pH Temperature(°C) <br /> oncentration Comments <br /> A B A B A B A B <br /> Control 10 10 1 9.20 9.10 7.43 7.46 19.4 1 19.4 1 Analyst: KR <br /> 250 mg/L 10 10 8.70 8.70 8.13 8.16 19.4 1 19.4 <br /> 500 mg/L 10 10 8.80 8.70 8.25 8.23 19.4 19.4 1 Date: 2/16/2016 <br /> 750 mg/L__L 10 10 I 8.70 1 8.60 1 8.26 8.24 I 19.4 1 19.4 1 Time: 11:30 AM <br /> Control 10 10 1 8.70 1 8.80 1 8.00 8.01 19.9 19.9 Analyst: DG <br /> 250 mg/L 10 10 7.00 7.20 7.41 7.60 19.9 19.9 <br /> 500 mg/L 10 10 7.90 7.90 7.58 7.59 19.9 1 19.9 Date: 2/17/2016 <br /> 750 mg/L 1 10 10 I 8.00 8.10 I 7.61 7.66 I 19.9 19.9 I Time: 10:30 AM <br /> Control 10 10 8.90 8.90 8.11 8.01 19.5 19.5 Analyst: DG <br /> 250 mg/L I 10 10 I 6.50 6.80 I 7.38 7.44 I 19.5 19.5 <br /> 500 mg/L 10 10 I 7.40 7.30 1 7.48 7.51 I 19.5 19.5 Date: 2/18/2016 <br /> 750 mg/L_L_ 10 10 I 7.30 1 7.80 1 7.60 7.63 I 19.5 1 19.5 1 Time: 4:00 PM <br /> Control 10 10 1 8.80 1 8.70 1 7.48 7.44 19.4 19.4 Analyst: KR <br /> 250 mg/L 10 10 I 6.20 1 7.70 1 7.24 7.51 I 19.4 19.4 1 <br /> 500 mg/L 10 10 7.30 7.90 7.47 7.58 19.4 19.4 Date: 2/19/2016 <br /> 750 mg/L 10 10 8.30 8.20 1 7.69 7.68 I 19.4 19.4 1 Time: 11:50 AM <br /> Control 10 10 8.90 8.90 8.20 8.14 19.5 19.5 Analyst: KR <br /> 250 mg/L 10 10 6.30 7.60 7.31 7.55 19.5 19.5 <br /> 500 mg/L 10 10 7.40 7.30 7.52 7.60 19.5 19.5 Date: 2/20/2016 <br /> 750 mg/L 10 10 8.00 8.20 7.70 7.72 19.5 19.5 Time: 12:00 PM <br /> Initial Final <br /> Control 750 mg/L Control 750 mg/L <br /> Hardness(mg/L as CaCO3) 46 47 55 58 <br /> Alkalinity(mg/L as CaCO3) 31 46 45 55 <br /> Conductivity(uS/cm) 176 188 201 256 <br /> Salinity(%o,ppt) N/A N/A N/A N/A <br /> Result:Mortality<40%at 750mg/L. Therefore LC50>=500mg/L('non-hazardous') <br /> 96 LC50: N/A LC50 Method: N/A <br /> 95%Upper Confident Limit: N/A 95%Lower Confident Limit: N/A <br /> CDPH ELAP 16441 NELAP 4033ORELAP DG Analyst's Initial Angela Rydelius,Lab Manager <br /> Page 4 of 9 <br />