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Enviro-Chem, Inc. 1214 E. Lexington Avenue, Pomona, CA 91766 Tel (909)590-5905 Fax (909)590-5907 Matrix: LIQ/sludge QAIQC Report Analysis Units Date Analyzed Sample I.D. S.R. Duplicate %RPD ACP%RPD Alkalinity mg/Kg 0.0% 0-20 Residual Chlorine mg/Kg 0.0% 0-20 EC umhos/cm 9/18/2012 120914-48 132.6 1334 0.6% 0-20 %Moisture/Total Solid 96 9/19/2012 120914-48 81.6 81.9 1.1% 0-20 r'I I pH units 4/29/2013 130429-9 6.85 6.86 1.1% 0-20 Density g/ml 9/19/2012 120914-48 113 1.13 0.00% 0-20 TSS mg/Kg 0.0% 0-20 Resistivity ohms 0.0% 0-20 BTU BTU/Ib 8/26/2009 090824-27 1 0 0 0.0% 0-20 %RPD= Relative Percent Difference ACP%RPD=Acceptable Relative Percent Difference 711.alysis finita I Date Analyzed Sample I.D. Spk Conc S.R. ACP%RPD RCP%RC MS MS%RC MSD MSD'/.RC %RPD Ammonia as N mg/Kg 6/25/2009 LCS1/2 5070 0.0 0-20 80-120 46.3 93% 48.] 96% 3.6% I\ABAS mg/Kg 30000.0 0.0 0-20 80-120 #VALUE! Chloride mg/Kg 200.0 0.0 0-20 80-120 #VALUE! COD mg/Kg� 500.0 0.0 0-20 80-120 #VALUE! 1664 mg/Kg 7/24/2012 LCS1/2 500.0 0.000 0-20 80-120 425 55% 430 66% 1.0% Cyari!d� mg/K9 5/1/2013 130429-8 10.0 0.0 0-20 80-120 8.53 85% 8.61 86% 0.8% Fluoride mg/Kg 1.0 0.0 0-20 80-120 #VALUE! Nitrate as N mg/Kg4.0 0.0 0-20 80-120 3.78 95% 3.81 95% 0.8% Nitrite as N mg/Kg 4.0 0.0 0-20 80-120 3.66 92% 3.74 94% 2.0% Oil and Grease mg/Kg 10/26/2009 LCS5/6 667 0 0-20 80-120 568 85% 576 86% 1.2% Phenolics mg/Kg 0.0 0-20 80-120 #VALUE! Sulfate mg/Kg 20.0 0.0 0-20 80-120 #VALUE! Sulfide Dissolved ma/Ka 9/18/2009 090915-1 3.0 fl.0 0-20 80-120 2.76 92% 2.72 91% 1.3% Sulfide.Reudive mg/K 5/1/2013 130429 3.0 0.0 0-20 80-120 2.67 89% 2.62 87% 1.7% TRPH mg/K 9/21/2009 LCS1/2 667 0.0 0-20 80-120 660 99% 660 99% 0.0% Formaldehyde mg/Kg 5/22/2009 LCS1/2 0.5 0.0 0-20 80-120 0.473 95% 0.484 97% 2.2% S.R. = Sample Results %RC = Percent Recovery ACP%RC =Accepted Percent Recovery Spk Conc=Spike Concentration Final Reviewer: Analyst Signature: A ~-