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Enviro-Chem, Inc. 1214 E. Lexington Avenue, Pomona, CA 91766 Tel (909)590-5905 Fax(909)590-5907 8270 QA/QC Report Matrix: Soil/Solid/Sludge/Oil unit: n, r � � Date Analyzed: 5/1/2013 Matrix Spike (MS)/Matrix Spike Duplicate (MSD) Spiked Sample Lab I.D.: 130501-LCS1/LCS2 Analyte SR spk conc MS %MS MSD %MSD %RPD ACP %MS ACP RPD Phenol 0.0 40.0 49.8 124% 41.4 104% 18% 50-150 _ 0-20 Pyrene 0.0 40.0 39.0 98% 32.9 82% 17% 50-150 0-20 Laboratory Control Spike (LCS): Analyte I spk conc LCS % RC ACP%RC Phenol 2.0 1.99 100% 75-125 1,4-Dichlorobenzene 2.0 2.02 101% 75-125 2,4-Dichloro henol 2.0 1.91 96% 75-125 Hexachlorobutadiene _ 2.0 2.41 120% 75-125 4-Chloro-3-methylphenol 2.0 2.18 109% 75-125 Fluoranthene 2.0 1 : 2.14 1 107% 75-125 Surrogate Recovery spk conc ACP% %RC %RC %RC %RC %RC %RC -/,RC Sample I.D. i MB 130429-081130429-0 130429-14 130429-15 2-Fluorophenol 40 f 25-121 ' 97% 53% 88% 72% 70% Phenol-d5 40 24-113 95% 50% 85% 76% 75% Nitrobenzene-d5 40 23-120 `,96% 53% 85% 71% 70% 2-Fluorobi hen I 40 30-115 99°f} 65% 85% 74% 70% 2,4,6-Tribromo henol 40 19-122 680/6 53% 70% 103°0 71% Terphenyl-d14 40 18-137 95% 72% 86% 82% 70% Surrogate Recove spk conc I ACP% °I°R %RC. %RC %RC %RC %,.RC `IoRC Sample I.D. _F 2-Fluorophenol 4C 25-121 Phenol-d5 40 24-113 Nitrobenzene-d5 40 23-120 2-Fluorobiphen I 40 30-115 2,4,6-Tribromo henol 4-0 19-122 Ter hen I-d14 40 18-137 Surrogate Recovery spk conc ACP% %PC %RC -%RC %RC %oRC %RC %RC Sample I.D. 2-Fluorophenol40 25-121 Phenol-d5 40 24-113 Nitrobenzene-d5 4C 23-120 2-Fluorobi hen I 40 30-115 2,4,6-Tribromo henol 40 19-122 I Terphenyl-d14 40 18-137 "=Surrogate fail due to matrix interference Note: LCS,MS,MSD are in control therefore results are in control. Analyzed and Reviewed By:_ { Final Reviewer: