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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)593-2212 <br /> email: lab.geo@att.net <br /> Report# Z311907 Project: 17405 Hwy 88, Lockford,Ca Date: 09/30/13 <br /> Jim Thorpe, Inc. Date Recd: 09/19/13 <br /> P.O Box 357 <br /> Lodi,CA 95241 <br /> Sample ID: Dispenser South at 2 <br /> Lab ID Sample Date/Time RL Method Analyte Result Units Notes Started <br /> 7_311907-03 9/19/2013 14:00 5.0 8260B 1,2-Dichloroethane ND ug/kg 9/26/13 12:19 <br /> 5.0 Benzene ND ug/kg <br /> 10.0 Di-isopropyl Ether(DIPE) ND ug/kg <br /> 400 Ethanol ND ug/kg <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND ug/kg <br /> 5.0 Ethylbenzene ND ug/kg <br /> 10.0 Ethylene dibromide ND ug/kg <br /> 10.0 Methyl cert-Butyl Ether(MTBE) ND ug/kg <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND ug/kg <br /> 200 tert-Butanol(TBA) ND ug/kg <br /> 5.0 Toluene ND ug/kg <br /> 5.0 Xylenes,total ND ug/kg <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Notes <br /> 1,2-Dichloroethane-d4 20.00 17.6 88% 72-132 <br /> 2-Bromo-I-Chloropropane 20.00 18.8 94% 71-134 <br /> 4-Bromofluorobenzene 20.00 19.4 97% 74-132 <br /> Sample ID: Dispenser North at 2 <br /> Lab ID Sample Date/Time RL Method Analyte Result Units Notes Started <br /> Z3I1907-04 9/19/2013 14:05 5.0 8260B 1,2-Dichloroethane ND ug/kg 9/26/13 12:19 <br /> 5.0 Benzene ND ug/kg <br /> 10.0 Di-isopropyl Ether(DIPE) ND ug/kg <br /> 400 Ethanol ND ug/kg <br /> 10.0 Ethyl tert-Butyl Ether(ETBE) ND ug/kg <br /> 5.0 Ethylbenzene ND ug/kg <br /> 10.0 Ethylene dibromide ND ug/kg <br /> 10.0 Methyl tert-Butyl Ether(MTBE) ND ug/kg <br /> 10.0 Tert-Amyl Methyl Ether(TAME) ND ug/kg <br /> 200 tert-Butanol(TBA) ND ug/kg <br /> 5.0 Toluene ND ug/kg <br /> 5.0 Xylencs,total ND ug/kg <br /> 1.0 GC/MS Gasoline ND mg/kg <br /> Surrogate Amnt Spiked Amnt Recovered %Recovery QC Limit% Surrogate Nates <br /> 1,2-Dichloroethane-d4 20.00 15.7 78% 72-132 <br /> 2-Bromo-l-Chloropropane 20.00 17.0 85% 71-134 <br /> 4-Bromofluorobenzene 20.00 18.0 90% 74-132 <br /> Certification 4 2585 <br />