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01-28-'13 14:33 FROM -SKS ENTERPRISES INC. <br />December 27, 2012 <br />SKS Enterprises <br />209-7593154 <br />Lab ID <br />Customer <br />Quality Control - Inorganic <br />T-213 P007 <br />: STK1251045 <br />:3-13071 <br />F-130 <br />Constituent <br />Method <br />Date/Ib <br />Type <br />units <br />Cone. <br />QC Data <br />DQO <br />Note <br />etals <br />An,enic <br />6010B <br />12/05/12:217890AC <br />CCB <br />ppm <br />0.0081 <br />0.01 <br />admium <br />6010B <br />12/05/12:217890AC <br />CCV <br />ppm <br />1.000 <br />102% <br />90-110 <br />CCB <br />ppm <br />0.00043 <br />0.005 <br />CCV <br />ppm <br />1.000 <br />107% <br />90-110 <br />CCB <br />00111 <br />0.00077 <br />1 0.005 <br />Chromium <br />601013 <br />12/05/12:217890AC <br />CCV <br />ppm <br />1.000 <br />103% <br />90-110 <br />CCB <br />ppm <br />0.0007 <br />0-01 <br />CCV <br />ppm <br />1.000 <br />107% <br />90-110 <br />CCB <br />p2m <br />-0,0008 <br />0101 <br />Copper <br />60109 <br />12/05/12:217890AC <br />CCV <br />ppm <br />1,000 <br />99.6 9b <br />90-110 <br />CCB <br />ppm <br />-0.0008 <br />0.01 <br />CCV <br />ppm <br />1.000 <br />103% <br />90-110 <br />CCB <br />I PPM <br />0.0007 <br />1 0.01 <br />Lead <br />60108 <br />12105/12:217890AC <br />CCV <br />ppm <br />L000 <br />104% <br />90-110 <br />CCB <br />ppm <br />0.0009 <br />0.01 <br />CCV <br />ppm <br />1.000 <br />110% <br />90-110 <br />CCB <br />RE <br />0.0043 <br />0.01 <br />ickel <br />601013 <br />1'2/05/12:217890AC <br />CCV <br />ppm <br />1.000 <br />104% <br />90110 <br />CCB <br />ppm <br />-0.0017 <br />0.01 <br />CCV <br />ppm <br />1.000 <br />108% <br />90-110 <br />CCB <br />PEM <br />-0.0008 <br />0.01 <br />Selenium <br />6010B <br />12/05/12:217890AC <br />CCV <br />ppm <br />1.000 <br />102% <br />90-110 <br />CCB <br />ppm <br />-0.0044 <br />0.01 <br />CCV <br />ppm <br />1.000 <br />109% <br />90-110 <br />CC13 I <br />Ppm <br />•0.0048 1 <br />0.01 <br />Zinc <br />6010B <br />12105/12:217890AC <br />CCV <br />ppm <br />1,000 <br />106% <br />90-110 <br />CCB <br />ppm <br />0.0027 <br />0.02 <br />CCV <br />ppm <br />1.000 <br />113% <br />90-110 <br />360 <br />CCB <br />m <br />0.0026 <br />0.02 <br />Mercury <br />7471 <br />12/05112:213466AC <br />Blank <br />mg/kg <br />ND <br />.0.03 <br />LCS <br />mg/kg <br />0.2500 <br />100% <br />85-115 <br />MS <br />mg/kg <br />0,2500 <br />107% <br />75-125 <br />(SP 1212292-001) <br />MSD <br />mg/kg <br />0.2500 <br />105% <br />75-125 <br />MSRPD <br />m0ke <br />0.2500 <br />1.2% <br />_'20 <br />et Chem <br />Solids <br />254OG <br />12/04/12:213459jam <br />Blank <br />% <br />ND <br />a0.1 <br />(STK1251045-002) <br />Du <br />% -- <br />1.6% <br />23.9 <br />Definition <br />PDS : PDS failed, matrix - Post Digestion Spike (PDS) not within Acceptance Range (AR) because of matrix intcrfcrcnces affecting this <br />analyte, <br />ICV : Initial Calibration Verification - Analyzed to verify the insttutticat calibration is within criteria. <br />ICE ; Initial Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />CCV : Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />CCB : Continuing Calibration Blank - Analyzed to verify the instrument baseline is within criteria. <br />Blank : Method Blank - Prepared to verify that the preparation pmccss is not contributing contamination to the samples. <br />LCS : Laboratory Control Standard/Sample - Prepared to verify that the preparation process is not affecting analyte recovery. <br />MS : Matrix Spikes - A random samples is spiked with a known amount of analyte. The recoveries are an indication of how that sample <br />matrix atfmts analyte recovery. <br />MSD : Matrix Spite Duplicate of MS/MSD pair - A random sample duplicate is spiked with a known amount of analyted. The recoveries <br />arc an indication of how that sample matrix affects analyte recovery. <br />Dup : Duplicate Sample - A random sample with each batch is prepared and analyzed in duplicate. The relative percent difference is an <br />indication of precision for the preparation and analysis. <br />MSRPD : MSIMSD Relative Percent Difference (RPD) - The MS rolative percent difference is an indication of precision for the preparation <br />and anal is. <br />Page 6 of 7 <br />Received Time Jan,28, 2013 1:36PM No.0447 <br />