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16TZIR Oilfield Environmental &Compliance, Inc. <br />CalRecycle Project: Lathrop <br />432 Geranium Circle Project Number: PNA-SWIS 39-22 PNA Lathrop Reported: <br />Galt CA, 95632 Project Manager: Sabra Ambrose 02/23/2018 15:39 <br />Polychlorinated Biphenyls by EPA Method 8082 - Quality Control <br />Analyte <br />Result <br />RL <br />Units Spike Source <br />Level Result <br />%REC %REC RPD RPD Notes <br />Limits Limit <br />Batch B8A0776 - EPA 8082 <br />Preparation: EPA 3550B 01/31/18 14:33 <br />0.0483 <br />0.020 mg/kg 0.0666 <br />Blank (B8A0776-BLK2) <br />54-105 <br />Analyzed: 02/01/18 19:19 <br />C-01 <br />PCB -1016 <br />ND <br />0.020 <br />mg/kg <br />PCB -1221 <br />ND <br />0.020 <br />" <br />10-210 <br />PCB -1232 <br />ND <br />0.020 <br />" <br />25.8 <br />PCB -1242 <br />ND <br />0.020 <br />" <br />Analyzed: 02/01/18 19:07 <br />PCB -1248 <br />ND <br />0.020 <br />" <br />0.0482 <br />PCB -1254 <br />ND <br />0.020 <br />" <br />PCB -1260 <br />PCB -1260 <br />ND <br />0.020 <br />" <br />30 <br />Surrogate: Decachlorobiphenyl <br />0.00733 <br />0.00833 <br />200833 <br />88.0 10-210 <br />Surrogate: 2,4,5,6 Tetrachloro-m-xylene 0.00466 <br />Surrogate: 2,4,5,6 Tetrachloro-m-xylene <br />0.00833 <br />55.9 10-161 <br />LCS (B8A0776-BS2) <br />Analyzed: 02/01/18 18:54 <br />C-01 <br />PCB -1016 <br />0.0483 <br />0.020 mg/kg 0.0666 <br />72.5 <br />54-105 <br />PCB -1260 <br />0.0534 <br />0.020 0.0666 <br />80.2 <br />58-126 <br />Surrogate: Decachlorobiphenyl <br />0.00754 <br />0.00833 <br />90.5 <br />10-210 <br />Surrogate: 2,4,5,6 Tetrachloro-m-xylene <br />0.00215 <br />0.00833 <br />25.8 <br />10-161 <br />LCS Dup (B8A0776-BSD2) <br />Analyzed: 02/01/18 19:07 <br />C-01 <br />PCB -1016 <br />0.0482 <br />0.020 mg/kg 0.0666 <br />72.3 <br />54-105 0.252 <br />30 <br />PCB -1260 <br />0.0564 <br />0.020 0.0666 <br />84.6 <br />58-126 5.34 <br />30 <br />Surrogate: Decachlorobiphenyl <br />0.00740 <br />0.00833 <br />88.8 <br />10-210 <br />Surrogate: 2,4,5,6 Tetrachloro-m-xylene <br />0.00330 <br />0.00833 <br />39.6 <br />10-161 <br />Duplicate (B8A0776-DUP2) <br />Source: 1800576-01 <br />Analyzed: 02/01/18 23:21 <br />PCB -1016 <br />ND <br />0.020 mg/kg ND <br />30 <br />PCB -1221 <br />ND <br />0.020 ND <br />30 <br />PCB -1232 <br />ND <br />0.020 ND <br />30 <br />PCB -1242 <br />ND <br />0.020 ND <br />30 <br />PCB -1248 <br />ND <br />0.020 ND <br />30 <br />PCB -1254 <br />ND <br />0.020 ND <br />30 <br />PCB -1260 <br />ND <br />0.020 ND <br />30 <br />Surrogate: Decachlorobiphenyl <br />0.00703 <br />0.00833 <br />84.4 <br />10-210 <br />Surrogate: 2,4,5,6 Tetrachloro-m-xylene <br />0.00459 <br />0.00833 <br />55.1 <br />10-161 <br />The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in its entirety. <br />Client Connect: client.oec.comlreports TEL: (805) 922-4772 <br />307 Roemer Way, Suite 300, Santa Maria, CA 934 www.oecusa.com FAX: (805) 925-3376 <br />Page 69 of 87 <br />