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Oilfield Environmental &Compliance, Inc.
<br />CalRecycle Project: Lathrop
<br />432 Geranium Circle Project Number: PNA-SWIS 39-22 PNA Lathrop Reported:
<br />Galt CA, 95632 Project Manager: Sabra Ambrose 02/23/2018 15:39
<br />EPA 1613B m - Quality Control
<br />Analyte Result RL Units Spike Source %REC %REC RPD RPD Notes
<br />Level Result Limits Limit
<br />Batch 5397644 - EPA 1613B m Preparation: NA 02/07/18 00:00
<br />Matrix Spike (5397644 -MS)
<br />Source: 1800597-02
<br />Analyzed: 02/15/18 00:00
<br />Octa CDF
<br />99.3
<br />9.98
<br />pg/g 100
<br />0.257
<br />99
<br />63-170
<br />Octa CDD
<br />102
<br />9.98
<br />100
<br />1.06
<br />101
<br />78-144
<br />1,2,3,7,8,9-HexaCDF
<br />107
<br />4.99
<br />100
<br />0.335
<br />107
<br />78-130
<br />1,2,3,6,7,8 -Hexa CDF
<br />111
<br />4.99
<br />100
<br />0.355
<br />111
<br />84-130
<br />1,2,3,4,6,7,8 -Hepta CDD
<br />102
<br />4.99
<br />100
<br />0.323
<br />102
<br />70-140
<br />1,2,3,4,6,7,8 -Hepta CDF
<br />100
<br />4.99
<br />100
<br />0.128
<br />100
<br />82-122
<br />1,2,3,4,7,8,9 -Hepta CDF
<br />100
<br />4.99
<br />100
<br />0.205
<br />100
<br />78-138
<br />1,2,3,4,7,8 -Hexa CDD
<br />95.1
<br />4.99
<br />100
<br />0.119
<br />95
<br />70-164
<br />1,2,3,7,8-PentaCDF
<br />103
<br />4.99
<br />100
<br />0.528
<br />102
<br />80-134
<br />1,2,3,6,7,8 -Hexa CDD
<br />107
<br />4.99
<br />100
<br />0.269
<br />107
<br />76-134
<br />1,2,3,7,8,9 -Hexa CDD
<br />109
<br />4.99
<br />100
<br />0.202
<br />109
<br />64-162
<br />1,2,3,7,8 -Penta CDD
<br />98.4
<br />4.99
<br />100
<br />0.351
<br />98
<br />25-181
<br />2,3,4,6,7,8 -Hexa CDF
<br />112
<br />4.99
<br />100
<br />0.371
<br />112
<br />70-156
<br />2,3,4,7,8 -Penta CDF
<br />112
<br />4.99
<br />100
<br />0.345
<br />112
<br />68-160
<br />2,3,7,8 -Tetra CDD
<br />82.3
<br />0.998
<br />100
<br />0.326
<br />82
<br />67-158
<br />2,3,7,8 -Tetra CDF
<br />105
<br />0.998
<br />100
<br />0.292
<br />105
<br />75-158
<br />1,2,3,4,7,8 -Hexa CDF
<br />104
<br />4.99
<br />100
<br />0.264
<br />104
<br />72-134
<br />Surrogate: C13-123478 HexaCDD
<br />90
<br />100
<br />90
<br />32-141
<br />Surrogate: C13-123478 HexaCDF
<br />91
<br />100
<br />91
<br />26-152
<br />Surrogate: 03-1234789 HeptaCDF
<br />82
<br />100
<br />82
<br />26-138
<br />Surrogate: C13-123678 HexaCDD
<br />89
<br />100
<br />89
<br />28-130
<br />Surrogate: C13-123678 HexaCDF
<br />91
<br />100
<br />91
<br />26-123
<br />Surrogate: C13-12378 PentaCDD
<br />77
<br />100
<br />77
<br />25-181
<br />Surrogate: C13-12378 PentaCDF
<br />74
<br />100
<br />74
<br />24-185
<br />Surrogate: 03-123789 HexaCDF
<br />80
<br />100
<br />80
<br />29-147
<br />Surrogate: 03-234678 HexaCDF
<br />83
<br />100
<br />83
<br />28-136
<br />Surrogate: 03-23478 PentaCDF
<br />77
<br />100
<br />77
<br />21-178
<br />Surrogate: C13-2378 TetraCDD
<br />19.8
<br />20
<br />99
<br />25-164
<br />Surrogate: C13-2378 TetraCDF
<br />16
<br />20
<br />80
<br />24-169
<br />Surrogate: C13-1234678 HeptaCDF
<br />94
<br />100
<br />94
<br />28-143
<br />Surrogate: C13-OCDD
<br />142
<br />200
<br />71
<br />17-157
<br />Surrogate: C13-1234678 Hep1aCDD
<br />89
<br />100
<br />89
<br />23-140
<br />Surrogate: 37CL4 2378 Tetra CDD
<br />17.2
<br />20
<br />86
<br />35-197
<br />The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must he reproduced in its entirety.
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