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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: Scrubber Ball Profile <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 01/25/2108:41 <br /> #1 Ball <br /> 2010171-01(Solid) <br /> Reporting Date Date <br /> Analyte Result Limit Units Batch Prepared Analyzed Method Notes <br /> Total Recoverable Metals <br /> Antimony 13.7 0.5 mg/kg A^J0284 10/26/20 10/26/20 EPA 6010B <br /> Arsenic 170 0.5 " " <br /> Barium 552 0.5 " " <br /> Beryllium ND 0.5 " <br /> Cadmium 10.2 0.5 " " <br /> Chromium 52.7 0.5 " <br /> Cobalt 2.1 0.5 " <br /> Copper 110 0.5 " <br /> Lead 779 0.5 " <br /> Molybdenum 1.4 0.5 " <br /> Nickel 8.5 0.5 " <br /> Selenium 1.1 0.5 " <br /> Silver ND 0.5 " <br /> Thallium ND 0.5 " <br /> Vanadium 33.2 0.5 " <br /> Mercury 8.80 1.60 A^J0292 10/26/20 10/26/20 EPA7471A R-07 <br /> STLC Metals <br /> Mercury ND 0.0160 mg/L A^K0018 11/02/20 11/02/20 EPA 7470A <br /> STLC Analysis <br /> Arsenic 0.2 0.2 mg/L A^K0058 11/05/20 11/05/20 EPA 6010B <br /> Chromium ND 0.2 <br /> Lead 0.8 0.2 " <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of10 <br />