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Mr. Lecil Colburn -2- 7 November 1990 <br /> through a more detailed analysis by a qualified professional . <br /> 2. Waste Characterization - The use of an MSDS is unacceptable because <br /> MSDS do not reveal concentrations of lead in a product which would <br /> cause it to be a "designated waste. " TCLP results are acceptable as <br /> an indicator of organic compound leaching potential , however a WET <br /> analysis must be done for elements or non-volatile compounds of <br /> concern. The WET and subsequent analysis for lead completed by Anlab <br /> had a detection limit of 1.0 mg/l , which is too high to adequately <br /> characterize lead concentrations in the Celotex wastes. The <br /> California Code of Regulations, Title 22 requires that EPA Method 7421 <br /> be used for lead analyses on WET extracts. Method 7421 has a <br /> detection limit of 0.001 mg/1 . <br /> 3. Volatile Organic Compounds - Chloroform has a water quality goal of <br /> 0.5 to 5 micrograms per liter (ug/1 ) . Multiplying this goal by the <br /> 100-fold attenuation factor and dividing by the TCLP dilution, which <br /> is 20, results in "designated" levels of 2.5 to 25 ug/1 . Since <br /> chloroform was found at 120 ug/l , chloroform would make the Celotex <br /> wastes a "designated waste" at the Corral Hollow Landfill . <br /> None of the laboratory tests looked for chlorofluorocarbons, even <br /> though MSDS indicate that sheathing contains 15% chlorofluorocarbons. <br /> 4. Representativeness of Samples - No rationale was presented concerning <br /> the ability of the single sample from the Tracy Celotex wastes to <br /> adequately rep_rqj=jthe waste stream proposed for disposal at Corral <br /> Hollow. Also, no"discussion of the materials analyzed by ARDL and <br /> 4uburban Laboratories was presented. Therefore, it is impossible to <br /> Aermine how these analyses represent the Tracy waste stream. <br /> 5. Maximum Contaminant Levels - EPA has proposed a new MCL for lead. <br /> Should this new MCL, 0.005 mg/1 , be approved, your analysis must be <br /> revised. <br /> 6. Dilution in Laboratory Tests - The WET results in a ten-fold dilution <br /> of the extract. Therefore, when calculating a "designated waste" <br /> level , the product of the water quality goal and the attenuation must <br /> be divided by the dilution factor. A dilution factor of 20 must be <br /> used with TCLP results. <br /> In order for the Regional Board to approve the disposal of Celotex wastes at the <br /> Corral Hollow Landfill , we require that you do the following tasks: <br /> 1. Representative sample(s) of the waste proposed for disposal at Corral <br /> Hollow Landfill must be analyzed for lead, chlorofluorocarbons and <br /> chloroform. Analysis for lead must be by the WET and must use the <br /> required Title 22 analyses. An explanation of any deviations from the <br /> required analyses must be included. <br />