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QC Sample Results Client: Patriot Environmental Services Job ID:440-250736-1 Project/Site: French Camp Method: 8260B -Volatile Organic Compounds (GC/MS) (Continued) Lab Sample ID: LCSD 440-571431/6 Client Sample ID: Lab Control Sample Dup Matrix: Solid Prep Type: Total/NA Analysis Batch: 571431 Spike LCSD LCSD %Rec. RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Trichloroethene 1000 888 ug/Kg 89 70-130 3 20 Trichlorofluoromethane 1000 867 ug/Kg 87 50-145 3 25 Vinyl chloride 1000 786 ug/Kg 79 10-120 2 30 1,2-Dibromoethane(EDB) 1000 889 ug/Kg 89 70-130 3 20 Bromochloromethane 1000 892 ug/Kg 89 65-125 2 20 Bromodichloromethane 1000 903 ug/Kg 90 65-135 4 20 Dibromochloromethane 1000 969 ug/Kg 97 65-140 3 20 p-Isopropyltoluene 1000 914 ug/Kg 91 70-125 3 20 2-Butanone(MEK) 5000 4210 ug/Kg 84 40-145 10 30 LCSD LCSD Surrogate %Recovery Qualifier Limits Toluene-d8(Surr) 107 60-140 4-Bromofluorobenzene(Surr) 103 65-140 Dibromofluoromethane(Surr) 99 55-140 --- — -----.............----------- Method: 8270C - Semivolatile Organic Compounds (GC/MS) Lab Sample ID: MB 440-570836/1-A Client Sample ID: Method Blank Matrix: Solid Prep Type: Total/NA Analysis Batch: 570955 Prep Batch: 570836 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac 1,2,4-Trichlorobenzene ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 1,3-Dichlorobenzene ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 1,4-Dichlorobenzene ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4,5-Trichlorophenol ND 500 200 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4,6-Trichlorophenol ND 500 160 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4-Dichlorophenol ND 250 50 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4-Dimethylphenol ND 250 98 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4-Dinitrophenol ND 1000 750 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,4-Dinitrotoluene ND 250 60 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2,6-Dinitrotoluene ND 250 71 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Chloronaphthalene ND 250 50 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Chlorophenol ND 250 52 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Methylnaphthalene ND 250 52 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Methylphenol ND 250 60 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Nitroaniline ND 250 170 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 2-Nitrophenol ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 3,3'-Dichlorobenzidine ND 500 110 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 3-Nitroaniline ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4,6-Dinitro-2-methylphenol ND 420 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Bromophenyl phenyl ether ND 250 56 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Chloro-3-methylphenol ND 400 150 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Chloroaniline ND 500 150 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Chlorophenyl phenyl ether ND 500 200 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 3-Methylphenol+4-Methylphenol ND 250 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Nitroaniline ND 500 100 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 4-Nitrophenol ND 1000 500 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 Acenaphthene ND 250 130 ug/Kg 09/25/19 14:06 09/26/19 09:44 1 Eurofins TestAmerica, Irvine Page 16 of 31 10/7/2019