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ZOOZ/ST/OT Report Number: 28968 <br />QC Report: Laboratory Control Sample (LCS) <br />Date: 10/15/2002 <br />Project Name: UNITED STORAGE <br />Project Number: A002-124-1 <br />Spike <br />Parameter Level Units <br />Analysis <br />Method <br />Date <br />Analyzed <br />LCS <br />Percent <br />Remy. <br />LCS <br />Percent <br />Recov. <br />Limit <br />TPH as Diesel 20.0 mg/Kg M EPA 8015 10/8/02 102 70-130 <br />Benzene 0.0396 mg/Kg EPA 8260B 10/9/02 102 70-130 <br />Toluene 0,0396 mg/Kg EPA 8260B 10/9/02 96.2 70-130 <br />Tert-Butanot 0,198 mg/Kg EPA 8260B 10/9/02 94.9 70-130 <br />Methyl-t-Butyl Ether 0.0396 mg/Kg EPA 8260B 10/9/02 87.7 70-130 <br />1 , 1-Dichloroethane 40.0 ug/L EPA 826013 10/7/02 92.9 70-130 <br />Benzene 40.0 ug/L EPA 8260B 10/7/02 94.8 70-130 <br />1 , 2-Dichloroe thane 40.0 ug/L EPA 8260B 1017/02 97.4 70-130 <br />Toluene 40.0 ug/L EPA 8260B 10/7/02 96.8 70-130 <br />Chlorobe nzene 40.0 ug/L EPA 82603 10/7/02 102 70-130 <br />Tert-Butan ol 200 ugIL EPA 8260B 10/7102 104 70-130 <br />Methyl-t-Butyl Ether 40.0 ug/L EPA 8260B 10/7/02 86.8 70-130 <br />1,1-Dichloroethane 40.0 ug/L EPA 8260B 10/7/02 97.8 70-130 <br />Benzene 40,0 ug/L EPA 82606 10/7/02 97.8 70-130 <br />1,2-Dichloroethane 40.0 ug/L EPA 8260B 10/7/02 99.9 70-130 <br />Toluene 40.0 ug/L EPA 8260B 10/7/02 99.0 70-130 <br />Chiorobe nzene 40.0 ug/L EPA 82608 10/7/02 106 70-130 <br />Tert-Butan ol 200 ug/L EPA 8260B 10/7/02 108 70-130 <br />Methyl-t-Butyl Ether 40.0 ug/L EPA 8260B 10/7/02 88.1 70-130 <br />16111 <br />KIPP ANALYTICAL, LLC <br /> Approved By: p4e1Kiff 1 <br />2795 2nd St, Suite 300 Davis, CA 95616 530-297-4800 8t2L.6ZOE9 1VOLLA7VNV AAIA