Laserfiche WebLink
Method blanks are run to check whether the glassware and reagents are free of <br />interference from chemicals that would invalidate the analyses; <br />Standards are prepared using the applicable reference materials; <br />Matrix spikes are analyzed in duplicate to validate the accuracy and precision of the <br />method; and <br />During groundwater sampling, a travel blank sample consisting of organic-free water <br />is prepared and containerized in the laboratory, transported to the site, and handled <br />and transported in the same manner as the groundwater samples. <br />Photo ionization Detector (PID) : The PD is calibrated in accordance with the manufacture's <br />recommendations prior to use in the field. Upon arrival at the project site, the PD is used to monitor <br />background concentrations of organic vapors in the atmosphere at the site. The background <br />concentrations are measured in a location upwind and removed as possible from sources of organic <br />vapors on the site. When background concentrations of organic vapors register as "0.0" on the PD, <br />subsequent readings of "0.0" registered from samples tested in the field are recorded as "0"(not <br />detected). When background concentrations of organic vapors register at some quantity above "0.0", <br />subsequent readings registered from samples tested in the field at or below this value are recorded <br />as "B/G" (background). <br />Decontamination Rinsate, Monitoring Well Purge Water, and Soil Cuttings Disposal: <br />The soil cuttings generated by drilling operations are retained on site, and either covered by plastic <br />sheeting or containerized in United States Department of Transportation (DOT)-approved drums or <br />lined, roll-on/roll-off dumpsters. The drilling equipment decontamination rinseate is also stored in <br />drums. Water purged from monitoring wells is containerized in drums if contamination is known <br />or suspected. Drums containing soil, rinsate, and purged water are sealed and temporarily stored on <br />site at a location remote to the public. Each drum is labeled to identify its contents. Disposal of <br />these wastes will be the responsibility of the client. The client will be informed that the wastes must <br />be disposed in accordance with applicable Federal, State, and local regulations. <br />Performing Head Space Analyses: Head space analysis is performed using a photo ionization <br />detector (HD) or a drager tube. A soil sample is placed in a sealed glass container or plastic bag, <br />agitated, and placed in a warm atmosphere. After approximately 15 minutes, which is generally <br />sufficient for some of the volatiles to escape from the soil, the PD probe or tip of the drager tube <br />is inserted into the container and the gas is sampled. The highest concentration of organic vapors <br />displayed by the ND or the drager tube reading will be recorded.