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'Naphthalene <11.28 <br />-Acenaphthylene <24.79 <br />' Acenaphthene <12.60 <br />I Fluorene <2.963 <br />LPhenanthrene <0.8033 <br />Anthracene <0.5808, <br />I <br />Benzo(k)fluoranthene <0.7904 <br />1 Indeno(1,2,3-cd)pyrene <0.8228 <br />%REC Limits <br />332.8 301.6 91 48-120 <br />665.6 595.4 89 36-120 <br />332.8 280.9 84 38-127 <br />66.56 59.47 89 36-137 <br />33.28 28.54 86 32-196 <br />33.28 26.79 80 55-160 <br />33.28 31.44 94 25-148 <br />33.28 31.15 94 43-181 <br />Analyte MSS Result Spiked : <br />surrog4„ oggamam%REc Limits <br />1 -Methylnaphthalene (UV) 92 47-124 <br />1-Methylnaphthalene (F) 92 46-127 <br />1-Methylnaphthalene (UV) <br />1-Methylnaphthalene (F) <br />99 47-124 <br />94 46-127 <br />Curtis & Tompkins, Ltd. <br />atch QC Report <br />Po lynuclear Aromatics by HPLC <br />ab #: 177317 Prep: EPA 3550B <br />'Client: Twining Laboratories, Inc. Analysis: EPA 8310 <br />IProject#: STANDARD <br />Batch#: 98694 <br />Sampled: 01/19/05 <br />Received: 01/25/05 <br />Prepared: 01/27/05 <br />Analyzed: 02/02/05 <br />Field ID: SB-1-4@0 <br />MSS Lab ID: 177317-001 <br />'Matrix: Soil <br />"Units: ug/Kg <br />Basis: as received <br />IDiln Fac: 1.000 <br />Type: MS Lab ID: QC280876 <br />7ype : MSD Lab ID: QC280877 <br />im <br />Naphthalene 333.9 318.9 95 48-120 5 34 <br />Acenaphthylene 667.8 614.2 92 36-120 3 31 <br />Acenaphthene 333.9 337.4 101 38-127 18 36 <br />Fluorene 66.78 66.86 100 36-137 11 36 <br />Phenanthrene , 33.39 29.77 89 32-196 4 68 <br />I Anthracene 33.39 28.20 84 55-160 5 52 <br />Benzo (k) fluoranthene 33.39 32.33 97 25-148 2 47 <br />Indeno (1,2,3 -cd) pyrene 33.39 31.93 96 43-181 2 54 <br />%REC Limits <br />RPD. Relative Percent Difference <br />Page 1 of 1