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tinalyte <br />Semi- atile Organics - Quality Cont <br />Result Reporting MDL Units Spike Source %REC %RUC <br />Limit Level Result Limits <br />RPD RPD <br />Limit <br />Batch T5A2114 - EPA 3550B _, <br />Matrix Spike Dup (T5A2114-MSD1) Source: 5A20004-06 Prepared: 01/21/05 Analyzed: 01/24/05 <br />tdrin 0.0620 0.050 mg/kg 0.0417 ND 149 60-151 10.2 20 <br />mma-BHC (Lindane) 0.0410 0.050 mg/kg 0.0417 ND 98.3 60-130 5.00 20 <br />Heptachlor 0.0370 0.050 mg/kg 0.0417 ND 88.7 55-135 8.45 20 <br />Batch T5A2115 - EPA 3550B L <br />Blank (T5A2115-BLK1) Prepared: 01/21/05 Analyzed: 01/24/05 <br /> <br />rrogate: Decachlorobtphenyl (DCB) 0.0320 0.010 mg/kg 0.0333 96.1 65-130 <br /> <br />13-1016 ND 0.10 mg/kg <br /> <br />PCB-1221 ND 0.10 mg/kg <br /> <br />-3B-1232 ND 0.10 mg/kg <br /> <br />13-1242 ND 0.10 mg/kg <br /> <br />PCB-1248 ND 0.10 mg/kg <br /> <br />°CB-1254 ND 0.10 mg/kg <br /> <br />13-1260 ND 0.10 mg/kg <br />LCS (T5A2115-BS1) Prepared: 01/21/05 Analyzed: 01/24/05 <br />rrrogate: Decachlorobiphenyl (DCB) 0.0310 0.010 mg/kg 0.0333 93.1 60-130 <br />-.13-1016 0.102 0.10 mg/kg 0.150 68.0 60-130 <br />PCB-1260 0.105 0.10 mg/kg 0.150 70.0 60-130 <br />7,S Dup (T5A2115-BSD1) Prepared: 01/21/05 Analyzed: 01/24/05 <br />....irrogate: Decachlorobiphenyl (DCB) 0.0340 0.010 mg/kg 0.0333 102 60-130 <br />PCB-1016 0.106 0.10 mg/kg 0.150 70.7 60-130 3.85 20 <br />13-1260 0.115 0.10 mg/kg 0.150 76.7 60-130 9.09 20 <br />.latrix Spike (T5A2115-MS1) Source: 5A20004-06 Prepared: 01/21/05 Analyzed: 01/24/05 <br />cnrrogate: Decachlorobiphenyl (DCB) <br />13-1016 <br />r..13-1260 <br />0.0320 0.010 <br /> <br />0.101 0.10 <br /> <br />0.100 0.10 <br />mg/kg 0.0333 96.1 60-130 <br />mg/kg 0.150 ND 67.3 60-130 <br />mg/kg 0.150 ND 66.7 60-130 <br />1"atrix Spike Dup (T5A2115-MSD1) Source: 5A20004-06 Prepared: 01/21/05 Analyzed: 01/24/05 <br />trrogate: Decachlorobiphenyl (DCB) 0.0320 0.010 mg/kg 0.0333 96.1 60-130 <br />PCB-1016 0.0994 0.10 mg/kg 0.150 ND 66.3 60-130 1.60 20 <br />"CB-1260 0.0986 0.10 mg/kg 0.150 ND 65.7 60-130 1.41 20 <br />Batch T5A2401 - EPA 3550B <br />Blank (T5A2401-BLK1) Prepared: 01/24/05 Analyzed: 01/25/05 <br />Trogate: 2,4,6-Tribromophenol 2.66 0.033 mg/kg 3.33 <br />,arrogate: 2-Fluorobiphenyl 1.25 0.033 mg/kg 1.67 <br />Surrogate: 2-Fluoropheno1 1.82 0.033 mg/kg 3.33 <br />frrogate: d14-Terphenyl 0.920 0.033 mg/kg 1.67 <br />rrrogate: Nitrobenzene-d5 1.09 0.033 mg/kg 1.67 <br />Surrogate: Phenol-d5 2.15 0.033 mg/kg 3.33 <br />2,4-Trichlorobenzene ND 0.33 mg/kg <br />3-Dinitrobenzene ND 0.33 mg/kg <br />1,4-Dichlorobenzene ND 0.33 mg/kg <br />' 4-Naphthoquinone ND 0.33 mg/kg <br />Naphthylamine ND 0.33 mg/kg <br />2,3,4,6-Tetrachlorophenol ND 0.33 mg/kg <br /> <br />79.9 10-200 <br /> <br />74.9 10-200 <br /> <br />54.7 10-200 <br /> <br />55.1 10-200 <br /> <br />65.3 10-200 <br /> <br />64.6 10-200