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Semi- atile Organics - Quality Cont Result Reporting MDL Units Limit Spike Level Source Result %REC %REC Limits RPD RPD Limit Batch T5A2401 - EPA 3550B LCS (T5A2401-BS1) Prepared: 01/24/05 Analyzed: 01/25/05 Chlorophenol 2.16 0.33 mg/kg 3.33 64.9 10-200 Chloro-3-methylphenol 2.73 0.33 mg/kg 3.33 82.0 10-200 Acenaphthene 1.20 0.33 mg/kg 1.67 71.9 10-200 Nitrosodi-n-propylamine 1.42 0.33 mg/kg 1.67 85.0 10-200 enol 2.48 0.33 mg/kg 3.33 74.5 10-200 Pyrene 0.900 0.33 mg/kg 1.67 53.9 10-200 -25 Dup (T5A2401-BSD1) Prepared: 01/24/05 Analyzed: 01/25/05 ...-rrogate: 2,4,6-Tribromophenol 3.54 0.033 mg/kg 3.33 106 10-200 Surrogate: 2-Fluorobiphenyl 0.980 0.033 mg/kg 1.67 58.7 10-200 rrogate: 2-Fluorophenol 1.75 0.033 mg/kg 3.33 52.6 10-200 rrogate: d14-Terphenyl 1.07 0.033 mg/kg 1.67 64.1 10-200 Surrogate: Nitrobenzene-d5 0.943 0.033 mg/kg 1.67 56.5 10-200 _ rrogate: Phenol-d5 2.20 0.033 mg/kg 3.33 66.1 10-200 !,4-Trichlorobenzene 0.658 0.33 mg/kg 1.67 39.4 10-200 15.0 20 1,4-Dichlorobenzene 0.658 0.33 mg/kg 1.67 39.4 10-200 9.83 20 ^ 4-Dinitrotoluene 1.49 0.33 mg/kg 1.67 89.2 10-200 5.52 20 Chlorophenol 2.01 0.33 mg/kg 3.33 60.4 10-200 7.19 20 4-Chloro-3-methylphenol 2.79 0.33 mg/kg 3.33 83.8 10-200 2.17 20 A ‘;enaphthene 1.08 0.33 mg/kg 1.67 64.7 10-200 10.5 20 Nitrosodi-n-propylamine 1.48 0.33 mg/kg 1.67 88.6 10-200 4.14 20 rnenol 2.39 0.33 mg/kg 3.33 71.8 10-200 3.70 20 Pvrene 0.955 0.33 mg/kg 1.67 57.2 10-200 5.93 20 atrix Spike (T5A2401-MS1) Source: 5A20004-06 Prepared: 01/24/05 Analyzed: 01/25/05 Surrogate: 2,4,6-Tribromophenol 3.51 0.033 mg/kg 3.33 105 10-200 rrogate: 2-Fluorobiphenyl 0.788 0.033 mg/kg 1.67 47.2 10-200 rrogate: 2-Fluorophenol 1.97 0.033 mg/kg 3.33 59.2 10-200 Surrogate: d14-Terphenyl 1.05 0.033 mg/kg 1.67 62.9 10-200 .currogate: Nitrobenzene-d5 0.901 0.033 mg/kg 1.67 54.0 10-200 rrogate: Phenol-d5 2.34 0.033 mg/kg 3.33 70.3 10-200 _,2,4-Trichlorobenzene ND 0.33 mg/kg 1.67 ND 10-200 1,4-Dichlorobenzene ND 0.33 mg/kg 1.67 ND 10-200 I.-Dinitrotoluene 1.50 0.33 mg/kg 1.67 ND 89.8 10-200 Thlorophenol 2.35 0.33 mg/kg 3.33 ND 70.6 10-200 4-Chloro-3-methylphenol 2.73 0.33 mg/kg 3.33 ND 82.0 10-200 :enaphthene 1.11 0.33 mg/kg 1.67 ND 66.5 10-200 Nitrosodi-n-propylamine 1.21 0.33 mg/kg 1.67 ND 72.5 10-200 Phenol 2.48 0.33 mg/kg 3.33 ND 74.5 10-200 Tene 0.901 0.33 mg/kg 1.67 ND 54.0 10-200 _ _atrix Spike Dup (T5A2401-MSD1) Source: 5A20004-06 Prepared: 01/24/05 Analyzed: 01/25/05 Surrogate: 2,4,6-Tribromophenol 3.51 0.033 mg/kg 3.33 105 10-200 rrogate: 2-Fluorobiphenyl 0.724 0.033 mg/kg 1.67 43.4 10-200 _ .rrogate: 2-Fluorophenol 1.94 0.033 mg/kg 3.33 58.3 10-200 Surrogate: d14-Terphenyl 1.00 0.033 mg/kg 1.67 59.9 10-200 rrogate: Nitrobenzene-d5 0.831 0.033 mg/kg 1.67 49.8 10-200 rrogate: Phenol-d5 2.27 0.033 mg/kg 3.33 68.2 10-200 1,2,4-Trichlorobenzene 0.169 0.33 mg/kg 1.67 ND 10.1 10-200 20