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Semi- .atile Organics - Quality Conti <br />Result Reporting NIDL Units Spike Source %REC <br />Limit Level Result <br />%REC <br />Limits <br />RPD RPD <br />Limit <br />Batch T5A2409 - EPA 3550B <br />Prepared: 01/24/05 Analyzed: 01/26/05 <br />0.0580 <br />0.0510 <br />0.0630 <br />0.0550 <br />1.0 <br />0.25 <br />0.25 <br />0.50 <br />mg/kg 0.0667 87.0 <br />mg/kg 0.0667 76.5 <br />mg/kg 0.0667 94.5 <br />mg/kg 0.0667 82.5 <br />70-130 <br />70-130 <br />70-130 <br />70-130 <br />1.74 <br />4.00 <br />1.57 <br />15.1 <br />20 <br />20 <br />20 <br />20 <br />Source: 5A20004-06 Prepared: 01/24/05 Analyzed: 01/26/05 <br />0.0610 5.0 mg/kg 0.0667 91.5 70-130 <br />0.0640 1.0 mg/kg 0.0667 ND 96.0 70-130 <br />0.0560 0.25 mg/kg 0.0667 ND 84.0 70-130 <br />0.0800 0.25 mg/kg 0.0667 ND 120 70-130 <br />0.0640 0.50 mg/kg 0.0667 ND 96.0 70-130 <br />Source: 5A20004-06 Prepared: 01/24/05 Analyzed: 01/26/05 <br />0.0600 5.0 mg/kg 0.0667 90.0 70-130 <br />0.0680 1.0 mg/kg 0.0667 ND 102 70-130 6.06 20 <br />0.0630 0.25 mg/kg 0.0667 ND 94.5 70-130 11.8 20 <br />0.0830 0.25 mg/kg 0.0667 ND 124 70-130 3.68 20 <br />0.0670 0.50 mg/kg 0.0667 ND 100 70-130 4.58 20 <br />Batch T5A2609 - EPA 3550B <br />Prepared: 01/26/05 Analyzed: 01/27/05 <br />0.232 0.10 mg/kg 0.400 58.0 0-200 <br />ND 3.5 mg/kg <br />ND 5.0 mg/kg <br />ND 2.5 mg/kg <br />Prepared: 01/26/05 Analyzed: 01/27/05 <br />0.416 0.10 mg/kg 0.400 104 0-200 <br />6.52 3.5 mg/kg 10.2 63.9 60-130 <br />32.7 5.0 mg/kg 36.0 90.8 65-130 <br />2.39 2.5 mg/kg 3.76 63.6 60-130 <br />Prepared: 01/26/05 Analyzed: 01/27/05 <br />0.414 0.10 mg/kg 0.400 104 0-200 <br />6.59 3.5 mg/kg 10.2 64.6 60-130 1.07 20 <br />32.0 5.0 mg/kg 36.0 88.9 65-130 2.16 20 <br />2.34 2.5 mg/kg 3.76 62.2 60-130 2.11 20 <br />Source: 5A20004-06 Prepared: 01/26/05 Analyzed: 01/27/05 <br />0.397 0.10 mg/kg 0.400 99.2 0-200 <br />3.98 3.5 QM-05 mg/kg 10.2 ND 39.0 60-130 <br />29.5 5.0 mg/kg 36.0 ND 81.9 65-130 <br />2.82 2.5 mg/kg 3.76 ND 75.0 60-130 <br />Source: 5A20004-06 Prepared: 01/26/05 Analyzed: 01/27/05 <br />0.379 0.10 mg/kg 0.400 94.8 0-200 <br />3.73 3.5 QM-05 mg/kg 10.2 ND 36.6 60-130 6.49 20 <br />27.9 5.0 mg/kg 36.0 ND 77.5 65-130 5.57 20 <br />2.72 2.5 mg/kg 3.76 ND 72.3 60-130 3.61 20 <br />I <br />tuaalyte <br />LCS Dup (T5A2409-BSD1) <br />ionazin <br />methoate <br />Diazinon <br />rathion-methyl <br />_ atrix Spike (T5A2409-MS1) <br />Surrogate: Triphenyl phosphate <br />ionazin <br />.....methoate <br />Diazinon <br />rathion-methyl <br />atrix Spike Dup (T5A2409-MSD1) <br />'-rrogate: Triphenyl phosphate <br />ionazin <br />uimethoate <br />niazinon <br />rathion-methyl <br />ank (T5A2609-BLK1) <br />..__ rrogate: o-Terphenyl <br />C6-C12 <br />3-C22 <br />3-C32 <br />LCS (T5A2609-BS1) <br />rrogate: o-Terphenyl <br />C13-C22 <br />,3-C32 <br />LCS Dup (T5A2609-BSD1) <br />- rrogate: o-Terphenyl <br />-C12 <br />C13-C22 <br />013-C32 <br />atrix Spike (T5A2609-MS1) <br />Surrogate: o-Terphenyl <br />-C12 <br />3-C22 <br />C23-C32 <br />latrix Spike Dup (T5A2609-MSD1) <br />rrogate: o-Terphenyl <br />C6-C12 <br />3-C22 <br />3-C32