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Excelchem Laboratories, Inc. <br />Ancon Environmental <br /> Project: Stockton Diesel Spill <br />570 Business Park Dr. Project Number: 1043326 <br /> Date Reported: <br />Lincoln, CA 95678 <br /> Project Manager: Nolan Ryan 08/07/20 16:16 <br />Total Petroleum Hydrocarbons by FIB - Quality Control <br />Analyte Result <br />ReEnrItiitng Spike Source %AEC RPD <br />Units Level Result %REC Limits RPD Limit Notes <br />Batch AAG0213 - EPA 8015Mod <br />Blank (A^G0213-BLKI) <br />TPH as Diesel <br />TPH as Motor Oil <br /> <br />Prepared & Analyzed: 07/27/20 <br /> <br />ND 1.00 mg/kg <br /> <br />ND 10.0 <br /> <br />LCS (A"G0213-BS1) <br /> Prepared & Analyzed: 07/27/20 <br />TPH as Diesel <br /> <br />79.8 1.00 mg/kg 100 79.8 70-130 <br />LCS (A^G0213-BS2) <br /> Prepared & Analyzed: 07/27/20 <br />TPH as Motor Oil 72.4 10.0 mg/kg 100 72.4 70-130 <br />LCS Dup (AAG0213-BSD1) <br /> Prepared & Analyzed: 07/27/20 <br />TPH as Diesel 76.8 1.00 mg/kg 100 76.8 70-130 3.83 30 <br />LCS Dup (A^G0213-BSD2) Prepared & Analyzed: 07/27/20 <br />TPH as Motor Oil <br /> 75.1 10.0 mg/kg 100 75.1 70-130 3.62 30 <br />Matrix Spike (AAG0213-MS1) <br /> Source: 2007152-02 Prepared & Analyzed: 07/27/20 <br />T'PH as Diesel <br /> 83.8 1.00 mg/kg 100 ND 83.8 70-130 <br />Matrix Spike Dup (AAG0213-MSD1) <br /> <br />Source: 2007152-02 Prepared & Analyzed: 07/27/20 <br />11'1-I as Diesel <br /> <br />72.2 1.00 mg/kg 100 ND 72.2 70-130 14.9 30 <br />Batch AAG0218 - EPA 8015Mod <br />Blank (AAG0218-BLKI) Prepared & Analyzed: 07/29/20 <br />TPH as Diesel ND 50.0 ugh1 <br />TPH as Motor Oil ND 500 <br />Excelchem Laboratories. Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br />custody docwnent This analytical report must be reproduced in its entirety. <br />Laboratory Representative Page 8 of 18