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Alpha Analytical,Inc. QC SUMMARY REPORT <br /> 255 Glendale Ave,#21 <br /> ALPHA <br /> ... Sparks,Nevada 89431 WO#: 2009002 <br /> ANALYTICAL INC. TEL:(775)355-1044 FAX-(775)355-0406 <br /> Website:invw.alpha-analytical.com 03-Sep-20 <br /> Client: Broadbent&Associates, Inc. <br /> Project: 20-08-150/PFJ 1017 TestCode: VOC W <br /> Sample ID: 2009001-02AMSD SampType: MSD TestCode: VOC_W Units: pg/L <br /> Client ID: BatchQC Batch ID: A11455 TestNo: SW8260C <br /> Prep Date: 9/2/2020 RunNo: 10053 SegNo: 290735 <br /> Analysis Date: 9/2/2020 <br /> SPK SPK RPD <br /> Analyte Result PQL Value Ref Val %REC Lowl-imit HighLimit Ref Val %RPD RPDLimit Qual <br /> Surr:1,2-Dichloroethane-d4 45.4 50 90.7 69.51 130.49 45.6 0 0 <br /> Surr:Toluene-d8 51.3 50 103 69.51 130.49 50.2 0 0 <br /> Sum 4-Bromofluorobenzene 44.7 50 89.4 69.51 130.49 44.8 0 0 <br /> Sample ID: 2009001-02AMS SampType: MS TestCode: VOC_W Units: pg/L <br /> Client ID: BatchQC Batch ID: Al 1455 TestNo: SW8260C <br /> Prep Date: 9/1/2020 RunNo: 10053 SegNo: 290671 <br /> Analysis Date: 9/1/2020 <br /> SPK SPK RPD <br /> Analyte Result PQL Value Ref Val %REC Lowl-imit HighLimit Ref Val %RPD RPDLimit Qual <br /> Methyl tert-butyl ether(MTBE) 67.1 2.5 50 15.5 103 54.8 155 <br /> Benzene 47.7 2.5 50 0 95.4 67.8 140 <br /> Toluene 46.2 2.5 50 0 92.4 67.2 131 <br /> Ethylbenzene 47.8 2.5 50 2.16 91.2 70.3 122 <br /> Xylenes,Total 93.2 2.5 100 0.48 92.7 61 131 <br /> Naphthalene 50.5 10 50 1.56 97.8 31.6 164 <br /> Surr: 1,2-Dichloroethane-d4 45.6 50 91.2 69.51 130.49 <br /> Surr:Toluene-d8 50.2 50 100 69.51 130.49 <br /> Surr:4-Bromofluorobenzene 44.8 50 89.7 69.51 130.49 <br /> Qualifiers: B Analyte detected in the associated Method Blank <br /> ND Not Detected at the Reporting Limit <br /> R RPD outside accepted recovery limits Page 5 of 8 <br /> S Spike Recovery outside accepted recovery limits <br />