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Page 13 of 19 <br /> e u rof i ns Quality Control - LCS/LCSD <br /> Calscience <br /> Kiff Analytical Date Received: 07/17/14 <br /> 2795 2nd Street, Suite 300 Work Order: 14-07-1129 <br /> Davis, CA 95618-6505 Preparation: EPA 625 <br /> Method: EPA 625 <br /> Project: Parcel 2A Page 3 of 3 <br /> Quality Control Sample ID Type Matrix Instrument Date Prepared Date Analyzed LCS/LCSD Batch Number <br /> 099-15-026-215 LCS Aqueous GC/MS SS 07/19/14 07/22/14 12:52 140719L07 <br /> 099-15-026-215 LCSD Aqueous GC/MS SS 07/19/14 07/22/14 13:10 140719L07 <br /> Parameter SSDike LCS Conc. LCS LCSD LCSD %Rec.CL ME CL RPD RPD CL Qualifiers <br /> Added %Rec. Conc. %Rec. <br /> Phenol 200.0 69.78 35 69.12 35 12-151 0-174 1 0-23 <br /> 2-Chlorophenol 200.0 160.7 80 156.8 78 45-135 30-150 2 0-18 <br /> N-Nitroso-di-n-propylamine 200.0 158.8 79 159.3 80 52-128 39-141 0 0-13 <br /> 1,2,4-Trichlorobenzene 200.0 130.2 65 129.3 65 42-120 29-133 1 0-21 <br /> Naphthalene 200.0 141.3 71 140.9 70 21-133 2-152 0 0-20 <br /> 4-Chloro-3-M ethyl phenol 200.0 140.4 70 144.2 72 20-150 0-172 3 0-40 <br /> Dimethyl Phthalate 200.0 167.5 84 168.1 84 0-112 0-131 0 0-20 <br /> Acenaphthylene 200.0 161.2 81 161.8 81 33-145 14-164 0 0-20 <br /> Acenaphthene 200.0 165.5 83 162.4 81 51-137 37-151 2 0-11 <br /> 4-Nitrophenol 200.0 34.26 17 37.55 19 20-150 0-172 9 0-40 ME <br /> 2,4-Dinitrotoluene 200.0 147.2 74 156.5 78 25-143 5-163 6 0-36 Y <br /> Fluorene 200.0 159.1 80 162.6 81 59-121 49-131 2 0-20 <br /> Pentachlorophenol 200.0 108.6 54 107.9 54 20-150 0-172 1 0-40 0 <br /> Pyrene 200.0 171.9 86 168.1 84 45-135 30-150 2 0-20 <br /> Butyl Benzyl Phthalate 200.0 180.4 90 171.2 86 0-152 0-177 5 0-20 <br /> Total number of LCS compounds: 15 <br /> Total number of ME compounds: 1 <br /> Total number of ME compounds allowed: 1 <br /> LCS ME CL validation result: Pass <br /> RPD:Relative Percent Difference. CL:Control Limits <br /> 7440 Lincoln Way,Garden Grove,CA 92841-1427 • TEL:(714)895-5494 • FAX:(714)894-7501 <br />