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eurofins <br /> Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgmt Co Group Number: 1334981 <br /> Reported: 09/24/12 at 10:56 AM <br /> Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these <br /> situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise <br /> specified in the method. <br /> All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless <br /> otherwise noted on the Analysis Report. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result LOQ** MDL Units %REC %REC Limits RPD RPD Max <br /> Batch number: B122621AA Sample number(s) : 6785308-6785310 <br /> Benzene N.D. 0.005 0.0005 mg/kg 100 94 80-120 6 30 <br /> Ethylbenzene N.D. 0.005 0.001 mg/kg 99 93 80-120 6 30 <br /> Toluene N.D. 0.005 0.001 mg/kg 99 93 80-120 6 30 <br /> Xylene (Total) N.D. 0.005 0.001 mg/kg 101 95 80-120 6 30 <br /> Batch number: 12256SLD026 Sample number(s) : 6785308-6785310 <br /> Acenaphthene N.D. 0.0017 0.00067 mg/kg 100 73-120 <br /> Acenaphthylene N.D. 0.0017 0.00033 mg/kg 104 67-120 <br /> Anthracene N.D. 0.0017 0.00033 mg/kg 104 61-122 <br /> Benzo(a)anthracene N.D. 0.0017 0.00067 mg/kg 99 64-124 <br /> Benzo(a)pyrene N.D. 0.0017 0.00067 mg/kg 107 66-122 <br /> Benzo(b)fluoranthene N.D. 0.0017 0.00067 mg/kg 116 60-126 <br /> Benzo(g,h,i)perylene N.D. 0.0017 0.00067 mg/kg 109 66-130 <br /> Benzo(k)fluoranthene N.D. 0.0017 0.00067 mg/kg 108 65-130 <br /> Chrysene N.D. 0.0017 0.00033 mg/kg 99 66-121 <br /> Dibenz(a,h)anthracene N.D. 0.0017 0.00067 mg/kg 115 69-129 <br /> Fluoranthene N.D. 0.0017 0.00067 mg/kg 100 68-119 <br /> Fluorene N.D. 0.0017 0.00067 mg/kg 111 66-125 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.0017 0.00067 mg/kg 114 66-122 <br /> 1-Methylnaphthalene N.D. 0.0017 0.00067 mg/kg 112 72-120 <br /> 2-Methylnaphthalene N.D. 0.0017 0.00067 mg/kg 117 57-132 <br /> Naphthalene N.D. 0.0017 0.00067 mg/kg 114 67-120 <br /> Phenanthrene N.D. 0.0017 0.00067 mg/kg 102 76-120 <br /> Pyrene N.D. 0.0017 0.00067 mg/kg 98 60-124 <br /> Batch number: 122560027A Sample number(s) : 6785308-6785310 <br /> C10-C36 N.D. 12. 3.9 mg/kg <br /> Total TPH N.D. 12. 3.9 mg/kg 79 64-122 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name %RBC %RSC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 12256SLD026 Sample number(s) : 6785308-6785310 UNSPK: 6785308 <br /> Acenaphthene 96 93 37-136 3 30 <br /> Acenaphthylene 95 88 29-133 8 30 <br /> Anthracene 96 97 73-115 2 30 <br /> Benzo(a)anthracene 95 94 32-135 0 30 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />