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Attachment B:Data Usability Summary and Laboratory Analytical Results(January 2008) <br /> • Comparability <br /> DATA USABILITY SUMMARY <br /> The following sections summarize the findings of the data evaluation process. The following is a <br /> summary of the data verification and validation qualifiers used in the data evaluation: <br /> ualifier Description <br /> E Indicates the reported value is estimated due to associated quality control <br /> (QC)results. <br /> J Indicates the reported value is an estimated concentration detected <br /> between the method detection limit(MDL)and limit of quantitation <br /> (LOQ). <br /> R Indicates the result is rejected because of deficiencies in the ability to <br /> meet QC criteria and cannot be used for decision making. <br /> U Indicates the analyte was analyzed for,but not detected above the level <br /> of the associated value. <br /> A summary of qualified data is provided in Table B-1. Data validation reason codes for all qualified data <br /> are also presented and defined on Table B-1. <br /> Precision and Accuracy <br /> The precision and accuracy of field and laboratory QC samples were evaluated. The calculated relative <br /> percent differences(RPDs)for field duplicate and MS/MSD pairs provided information on the precision <br /> of sampling and analytical procedures, and the RPDs for laboratory control sample/laboratory control <br /> sample duplicate(LCS/LCSD)pairs provided information on the precision of the analytical procedures. <br /> Evaluation of the percent recoveries(%Rs) of MS/MSDs,LCS/LCSDs, and surrogates provided <br /> information on accuracy. <br /> MSIMSDs <br /> Project-specific MS/MSDs were collected with the groundwater samples. All MS/MSD samples were <br /> within QC range,with the following exceptions: MW6-W-080129MS and MW6-W-080129MSD had <br /> benzo(a)pyrene(46 and 54 micrograms per liter [gg/L]), indo(1,2,3-cd)pyrene(67 gg/L), and <br /> benzo(g,h,i)perylene(54 and 64 gg/L)below the acceptance criteria. Associated samples MW-2-W- <br /> 080129 MW-3-W-080129,MW-5-W-080129,MW-6-W-080129,MW-6WD-W-080129, and MW-7-W- <br /> 080129 will be flagged E for specific analytes. <br /> LCS/LCSDs <br /> A LCS was analyzed with each analytical batch of samples. All LCS/LCSD%Rs were within the <br /> laboratory control limits. <br /> Surrogates <br /> All surrogates were within QC criteria. <br /> Representativeness <br /> Representativeness was assessed through the evaluation of the equipment blank sample, chain-of-custody <br /> forms,preservation, and holding times. The reported results were also compared to the laboratory's <br /> MDLs and LOQs. <br />