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California Laboratory Services <br /> Analysis Report: CAM17TTLC Metals, EPA Methods 6010/7000 <br /> Client; WHF Environmental Consultants Project No. : <br /> P.O. Box 427 Contact: Bill Fox <br /> Oakdale, CA 95361 Phone: (209) 848-4280 <br /> Project: US CAN COMPANY Lab Contact: Larry Mooney <br /> Job No. : 801043 <br /> Date Diyested: 12/14/95 COC Log No. : NO NUMBER <br /> Date Analyzed: 12/19/95 Lab ID No- : 241043 <br /> Date Reported: 12/20/95 Batch No. : M951214C <br /> Matrix: SOIL <br /> —.�_ -- ----- - MATRIX SPIKE -- --. ----- <br /> MS <br /> MS Conc. Recovery <br /> Analyte CAS No. (mg/kg) (percent) <br /> Ag (Si-Aver) '1440-22-4 20.0 87 <br /> As (Arsenic) 7410-38-2 8 .00 57 MA <br /> Ba (Barium) 7440-39--3 400 89 <br /> Be (Beryllium) 7440-41-'7 10.0 B5 <br /> Cd (Cadmium) '7440-43-9 10.0 78 <br /> ,.,.j Co (Cobalt) 7440 .48-4 LOU 85 <br /> Cr (Chromium) 7440-47-3 40.0 79 <br /> ;( Cu (Copper) 7440-50-8 50.0 84 <br /> H9 (Mercury) '?439-97-6 0.500 108 <br /> Mo (Molybdenum) '7439-98-7 100 83 <br /> Ni (Nickel) 7440 -02-0 100 32 <br /> Pb (Lead) 7439-92-1 100 82 <br /> Sb (Antimony) 7440 36-0 100 72 MA <br /> Se (Selenium) ?,7F,3-00-8 4 .00 28 MA <br /> T1 (Thallium) 7440--28-0 400 80 <br /> V (Vanadium) 744E-62-2 100 81 <br /> Za (Zinc) 7440--66-6 100 90 <br /> MA = Recovery data is outside standard QC Limits due to matrix <br /> interference. LCS recovery data validates methodology. <br /> rrta <br /> MATRIX SPIKE DUPLICATE <br /> MSN <br /> M:7f.; Colic-, Recovery <br /> Analyte CAs No. (mg/kg) (percent) <br /> Ag (Silver) '/440 -22-4 20.0 88 <br /> As (Arsenic) i'IAG- B 2 8 .00 43 MA <br /> Ba (Barium) 7.140-39-3 400 85 <br /> Be (Beryllium) 7440 . 41-'1 10.0 86 <br /> Cd (Cadraium, 7440 43-9 10.0 79 <br /> Cc (Cobalt) 7440-48--4 100 62 <br /> Cr (Chromium) 7440 -47-3 40.0 311 <br /> Cu (Copper) 74.10-50-8 50.0 82 <br /> Hy (Mercury) 7439 -97-6 0 .500 107 <br /> mci (Molybdenwa) 7439-98-7 1Gri 84 <br /> Ni (Nickel) 7440-02-0 100 83 i <br /> PU (Lead) 74-39- 92- 1 100 85 I! <br /> Sb (Antimony) 7440-36-0 100 75 <br /> Se (Selenium) '083--00--8 4 -00 34 MA <br /> T1 (Thallium[) 7440-28-0 400 81 <br /> V (Vanadium) 7,440 -6172- 2 100 85 <br /> Zri (Zinc) `.4.40-tab-6 100 84 <br /> MA = Recovery data is nurs:i6e sLnward S):.' limiLs due to matrix <br /> interference. LCS recovery Ai it:.fa validat us [[;eLhoaology. <br /> _c. DOME) ELAY 123L <br /> 3249 Fitzgerald Road Rancho C0M5va, + A -35742 (916) 6,87301 fax (916) 638.4510 <br />