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Soil samples for low- or non-volatile compounds as TPHd, TPHo, SVOCs, metals, PCBs and <br />pH will be collected using the remaining soil within the first sample sleeve. The exposed ends of <br />the sleeve will be capped with Teflon sheeting and secured with plastic end caps. The sample <br />will then be labeled, placed into a re-sealable plastic bag, and put into the insulated chest filled <br />with ice pending transport to a California certified laboratory for analysis. If insufficient soil <br />sample is collected, either an additional sample will be collected from the borehole beginning <br />where the last sample was collected, or the rig will be moved over three (3) feet from the initial <br />borehole and sampling will continue at the target depth. <br />Soil from the second (middle) sleeve will be placed into a re-sealable plastic bag and set aside <br />for approximately two (2) to five (5) minutes, after which time a measure of VOCs will be made <br />using a portable PD or equivalent organic vapor analyzer. The soil will then be described by a <br />California Professional Geologist, in accordance with the USCS method of soil description. Logs <br />of the boreholes will be prepared by or under the direct supervision of the Professional Geologist <br />responsible for this project. <br />During sampling, a mobile laboratory may be used to analyze the samples directly onsite. If <br />used, additional sampling may be advanced at other locations to further delineate petroleum <br />hydrocarbons and/or VOCs that exceed regulatory limits. The necessity for additional sampling <br />at other locations may also be indicated by high VOC measurements on the PD. The selection of <br />additional sample locations will be at the discretion of the Professional Geologist responsible for <br />this project. <br />Collected soil samples will be analyzed at different depths for one or more of the following: <br />TPHg, in accordance with Modified EPA Method 8015 and Method 5035 <br />preservation; <br />TPHd and TPHo, in accordance with Modified EPA Method 8015B; <br />VOCs, in accordance with EPA Method 8260B and Method 5035 preservation; <br />SVOCs, in accordance with EPA Method 8270C / 8310 (PAHs); <br />PCBs, in accordance with EPA Method 8082; <br />PH, in accordance with EPA Method 9040 / 9045; and <br />Total metals (no hexavalent chrome), in accordance with EPA Method 7470 / 7471. <br />Soluble metals, in accordance with WET, may be performed for those samples where <br />the TTLC12 concentration exceeds 10x the STLC I3 limit. <br />Although six (6) soil samples will be collected at each grid sample location, the samples <br />initially will not be analyzed for the above PCOCs and COCs. Instead, a systematic analytical <br />12 Total Threshold Limit Concentration (regulatory limit that defines a characteristic of hazardous waste) <br />13 Soluble Threshold Limit Concentration (regulatory limit that defines a characteristic of hazardous waste) <br />Golden State Environmental, Inc. - 22 - Los Angeles, San Diego and Houston <br />Revised Work Plan — Soil and GW Characterization July 2006