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f------ PROVIDING QUALITY ANAI I I It Al. SERVICES NATIONWIDE <br />\ SunStar <br /> Laboratories, Inc. <br />25712 Commercentre Drive <br />Lake Forest, California 92630 <br />949.297.5020 Phone <br />949.297.5027 Fax <br />Krazan, Clovis Project: Wilson Way Property <br />215 West Dakota Avenue Project Number: 014-13157 <br /> Reported: <br />Clovis CA, 93612 <br /> Project Manager: Mike Bowery 08/23/13 17:12 <br />Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br />SunStar Laboratories, Inc. <br />Analyte Result <br />Reporting <br />Limit Units <br />Spike Source <br />Level Result %REC <br />%REC <br />Limits RPD <br />RPD <br />Limit Notes <br />Batch 3081221 - EPA 3550 ECD/GCMS <br />Blank (3081221-BLK1) Prepared: 08/12/13 Analyzed: 08/16/13 <br />Surrogate: 2-Fluorophenol 808 ug/kg 1670 48.5 14.3-83.1 <br />Surrogate: Phenol-d6 913 1670 59.8 12-95.6 <br />Surrogate: Nitrobenzene-d5 843 1670 50.6 21.3-119 <br />Surrogate: 2-Fluorobiphenyl 968 1670 58.1 32.4-102 <br />Surrogate: 2,4,6-Tribromophenol 850 FP 1670 51.0 18.1-101 <br />Surrogate: Terphenyl-d14 852 1670 51.1 29.1-130 <br />LCS (3081221-BS1) Prepared: 08/12/13 Analyzed: 08/16/13 <br />Phenol 1130 1000 ug/kg 1670 68.0 25.9-102 <br />2-Chlorophenol 974 1000 1670 58.5 37.1-110 <br />1,4-Dichlorobenzene 846 300 II 1670 50.8 36-97 <br />N-Nitrosodi-n-propylamine 1200 300 II 1670 72.0 30.8-81.8 <br />1,2,4-Trichlorobenzene 934 300 " 1670 56.1 39-98 <br />4-Chloro-3-methylphenol 1080 1000 " 1670 64.9 33.1-109 <br />Acenaphthene 1050 300 " 1670 62.8 38.9-79.4 <br />4-Nitrophenol 1460 1000 ,, 1670 87.4 14-103 <br />2,4-Dinitrotoluene 1070 300 ,, 1670 64.0 24-96 <br />Pentachlorophenol 908 1000 ,, 1670 54.5 8.05-120 <br />Pyrene 941 300 ,, 1670 56.5 25-85.2 <br />Surrogate: 2-Fluorophenol 827 1670 49.7 14.3-83.1 <br />Surrogate: Phenol-d6 1030 1670 61.9 12-95.6 <br />Surrogate: Nitrobenzene-d5 899 1670 53.9 21.3-119 <br />Surrogate: 2-Fluorobiphenyl 1050 1670 63.2 32.4-102 <br />Surrogate: 2,4,6-Tribromophenol 1000 1670 60.3 18.1-101 <br />Surrogate: Terphenyl-d14 882 1670 52.9 29.1-130 <br />LCS Dup (3081221-B5D1) Prepared: 08/12/13 Analyzed: 08/16/13 <br />Phenol 1200 1000 ug/kg 1670 72.2 25.9-102 6.00 42 <br />2-Chlorophenol 1040 1000 1670 62.2 37.1-110 6.17 40 <br />1,4-Dichlorobenzene 816 300 " 1670 49.0 36-97 3.58 28 <br />N-Nitrosodi-n-propylamine 1060 300 ,, 1670 63.3 30.8-81.8 12.8 38 <br />1,2,4-Trichlorobenzene 945 300 1670 56.7 39-98 1.13 28 <br />4-Chloro-3-methylphenol 1190 1000 ,, 1670 71.5 33.1-109 9.83 42 <br />Acenaphthene 1120 300 ,, 1670 67.3 38.9-79.4 6.92 31 <br />4-Nitrophenol 1100 1000 " 1670 66.0 14-103 27.9 50 <br />2,4-Dinitrotoluene 819 300 ,, 1670 49.1 24-96 26.3 38 <br />SunStar Laboratories, Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br />C414,7s <br />custody document. This analytical report must be reproduced in its entirety. <br />Daniel Chavez, Project Manager Page 87 of 90