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File Report <br />April 7, 1998 <br />locations during the owner's investigation into the vapor recovery system problem, RCP <br />determined that it should quickly identify any problems associated with the referenced <br />localized surface spill. <br />On March 13, 1998, Amherst's geologist collected two shallow soil samples from the <br />area identified by the SJCEHD as the entry point of the surface spill (lowest point where <br />the reported hydraulic pumping occurred). A small portion of the concrete apron in this <br />settled area was lifted out by hand and an undisturbed sample collected at the concrete <br />soil interface. The geologist then hand excavated down to a depth of 1.5 feet below the <br />concrete soil interface where a second undisturbed sample was collected <br />(see Figure 2). Given the closed status of the facility, these samples were collected to <br />determine a "worst case scenario" of the impact due to the diesel spill identified in <br />September 1997. The following procedures were used and maintained in the collection <br />of these two samples. <br />Undisturbed Soil Sample Collection <br />The undisturbed soil samples were collected per California Code of Regulations, Title <br />23, Section 2654, Subsection C. <br />A hand-driven sampler coupled with a stainless steel sleeve was used to collect <br />undisturbed soil samples. Once the desired depth for sampling was reached, a hand <br />sampler was driven to the desired depth, the sleeve removed from the sampler, the ends <br />sealed with Teflon followed by airtight plastic caps, and placed in an ice-chilled cooler for <br />preservation. Strict chain-of-custody forms were maintained to document the sample <br />collection and transportation to the laboratory for analysis. <br />Analytical Laboratory Analysis <br />These two samples were submitted to Sequoia Analytical (a California State Certified <br />Laboratory) for chemical analysis for total petroleum hydrocarbons as diesel by modified <br />EPA method 8015 and for Gasoline, benzene, toluene, ethylbenzene, and xylene by <br />4 <br />RCP0407