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1702619 <br />134125 <br />730392392; Lodi MCP-W Tokay <br />Client: Langan <br />Date Prepared: 2/13/17 <br />Date Analyzed: 2/13/17 <br />Instrument: GC18 <br />Matrix: Water <br />Project: <br />WorkOrder: <br />BatchID: <br />Extraction Method: SW5030B <br />Analytical Method: SW8260B <br />Unit: <br />Sample <br />- <br />Sample ID: MB/LCS-134125 <br />1702599-001AMS/MSD <br />McCampbell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mccampbell.com <br /> <br />Quality Control Report <br />QC Summary Report for SW8260B <br />Analyte MB <br />Result <br />LCS <br />Result <br />RL SPK <br />Val <br />MB SS <br />%REC <br />LCS <br />%REC <br />LCS <br />Limits <br />Tetrachloroethene ND 0.50 <br />1,2,3-Trichlorobenzene ND 0.50 <br />1,2,4-Trichlorobenzene ND 0.50 <br />1,1,1-Trichloroethane ND 0.50 <br />1,1,2-Trichloroethane ND 0.50 <br />Trichloroethene ND 10.8 0.50 10 108 43-157 <br />Trichlorofluoromethane ND 0.50 <br />1,2,3-Trichloropropane ND 0.50 <br />Vinyl Chloride ND 0.50 <br />Surrogate Recovery <br />Dibromofluoromethane 24.26 24.6 25 97 98 70-130 <br />Toluene-d8 23.37 23.9 25 93 95 70-130 <br />4-BFB 2.632 2.61 2.5 105 104 70-130 <br />Analyte MS <br />Result <br />MSD <br />Result <br />SPK <br />Val <br />SPKRef <br />Val <br />MS <br />%REC <br />MSD <br />%REC <br />MS/MSD <br />Limits <br />RPD RPD <br />Limit <br />Chlorobenzene 10.1 9.84 10 ND 101 98 77-120 2.42 20 <br />1,2-Dibromoethane (EDB) 107 10.5 10 ND 107 105 76-135 1.74 20 <br />1,2-Dichloroethane (1,2-DCA) 9.77 9.75 10 ND 98 98 73-139 0 20 <br />1,1-Dichloroethene 10.2 10.2 10 ND 102 102 59-140 0 20 <br />Trichloroethene 10.1 10.2 10 ND 101 102 64-132 0.119 20 <br />Surrogate Recovery <br />Dibromofluoromethane 24.5 24.6 25 98 98 73-131 0 20 <br />Toluene-d8 23.9 24.0 25 95 96 72-117 0.487 20 <br />4-BFB 2.39 2.34 2.5 96 94 74-116 1.99 20 <br />QA/QC Officer <br />Page 8 of 12 <br />NELAP 40330RELAP