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WG1600283 QUALITY CONTROL SUMMARY ONE LAB.NATIONWIDE. <br /> Metals (ICP) by Method 60108 L1300503-01 <br /> L1300676-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) <br /> (OS)L1300676-03 01/06/2121:58•(MS)R3610345-5 01/06/2122:08•(MSD)R3610345-6 01/06/2122:11 FC P <br /> Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec.Limits MS Qualifier MSD Qualifier RPD RPD Limits <br /> Analyte mg/kg mg/kg mg/kg mg/kg % % % % % TC <br /> Antimony 100 2.26 37.9 38.1 35.6 35.8 1 75.0-125 J6 J6 0.643 20 <br /> Arsenic 100 3.42 101 102 97.1 98.1 1 75.0-125 1.02 20 3 <br /> Ss <br /> Barium 100 73.4 156 162 82.5 88.5 1 75.0-125 3.79 20 <br /> Beryllium 100 6.48 100 102 93.9 95.6 1 75.0-125 1.73 20 Fn Cadmium 100 U 91.9 93.2 91.9 93.2 1 75.0-125 1.35 20 <br /> Chromium 100 366 403 444 36.7 78.1 1 75.0-125 J6 9.78 20 <br /> Cobalt 100 0.148 105 106 105 106 1 75.0-125 1.26 20 Fr Copper 100 1970 8750 6880 6790 4920 1 75.0-125 E V E J3 V 23.9 20 <br /> Lead 100 23.9 144 134 120 110 1 75.0-125 7.10 20 <br /> Molybdenum 100 3.80 96.8 97.5 93.0 93.7 1 75.0-125 0.653 20 <br /> Nickel 100 4.19 109 113 105 108 1 75.0-125 3.02 20 <br /> Selenium 100 3.26 90.1 91.0 86.9 87.7 1 75.0-125 0.951 20 FG1 <br /> Silver 20.0 U 20.4 20.7 102 104 1 75.0-125 1.51 20 <br /> Thallium 100 0.456 89.9 91.2 89.4 90.7 1 75.0-125 1.48 20 s <br /> Vanadium 100 8.80 100 102 91.2 93.3 1 75.0-125 1.98 20 AI <br /> Zinc 100 24600 24000 24200 0.000 0.000 1 75.0-125 E V E V 0.952 20 <br /> FSCI <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc USE#160805 L1300503 01/07/2114:44 9 of 15 <br />