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October 19, 2021 Lab ID : STK2154077 <br /> San Joaquin Co. Environmental Health Dep Customer : 3-17919 <br /> Quality Control - Inorganic <br /> Constituent Method Date/ID Type Units Conc. QC Data DQO Note <br /> Wet Chem <br /> Nitrate 300.0 (STK2154075-001) MSD mg/L 40.00 107% 85-119 <br /> MSRPD mg/L 10.00 6.2% <19 <br /> 300.0 10/01/21:215448njb CCB mg/I 0.00 0.5 <br /> CCV mg/I 20.00 104% 90-110 <br /> CCB mg/1 0.00 0.5 <br /> CCV m I 20.00 104% 90-110 <br /> Nitrate+Nitrite as N 300.0 10/01/21:211396NJB Blank mg/L ND <0.1 <br /> Nitrate Nitrogen 300.0 10/01/21:211396NJB Blank mg/L ND <0.1 <br /> Nitrite 300.0 10/01/21:211396NJB Blank mg/L ND <0.5 <br /> LCS mg/L 15.00 107% 90-110 <br /> MS mg/L 30.00 103% 74-126 <br /> (STK2154077-001) MSD mg/L 30.00 112% 74-126 <br /> MSRPD mg/L 10.00 8.0% <_20 <br /> MS mg/L 30.00 104% 74-126 <br /> (STK2154075-001) MSD mg/L 30.00 111% 74-126 <br /> MSRPD mg/L 10.00 6.7% 1 <20 <br /> 300.0 10/01/21:215448njb CCB mg/I 0.00 0.5 <br /> CCV mg/l 15.00 107% 90-110 <br /> CCB mg/1 0.00 0.5 <br /> CCV mg/1 15.00 108% 90-110 <br /> Nitrite Nitrogen 300.0 10/01/21:211396NJB Blank m ND <0.2 <br /> Sulfate 300.0 10/01/21:211396NJB Blank mg/L ND <0.5 <br /> LCS mg/L 50.00 107% 90-110 <br /> MS mg/L 100.0 102% 82-124 <br /> (STK2154077-001) MSD mg/L 100.0 110% 82-124 <br /> MSRPD mg/L 10.00 8.1% <23 <br /> MS mg/L 100.0 102% 82-124 <br /> (STK2154075-001) MSD mg/L 100.0 109% 82-124 <br /> MSRPD m 10.00 6.5% <23 <br /> 300.0 10/01/21:215448njb CCB mg/1 0.139 0.5 <br /> CCV mg/1 50.00 108% 90-110 <br /> CCB mg/1 0.00 0.5 <br /> CCV mg/1 50.00 108% 90-110 <br /> MBAs 5540C 10/01/21:215464jba CCB mg/l -0.0611 0.25 <br /> CCV mg/1 1.000 104% 90-110 <br /> CCB mg/I -0.0611 0.25 <br /> CCV m I 1.000 104% 1 90-110 <br /> MBA S Extraction 5540C 10/01/21211493jba Blank mg/L ND <0.1 <br /> LCS mg/L 0.5000 104% 86-114 <br /> BS mg/L 0.5000 95.0% 86-114 <br /> BSD mg/L 0.5000 99.3% 86-114 <br /> BSRPD mg/L 0.5000 4.5% <5 <br /> Definition <br /> ICB :Initial Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. <br /> CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. <br /> Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. <br /> LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. <br /> MS Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample <br /> matrix affects analyte recovery. <br /> MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyte.The recoveries <br /> are an indication of how that sample matrix affects analyte recovery. <br /> BS :Blank Spikes-A blank is spiked with a known amount of analyte.It is prepared to verify that the preparation process is not <br /> affecting analyte recovery. <br /> Page 8 of 9 <br />