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Analyte Result mg/kg Qualifier MDL mg/kg RDL mg/kg Dilution Analysis date/time Batch 1,2-Dibromo-3-Chloropropane U 0.00390 0.0250 1 01/14/202117:40 WG1605648 1,2-Dibromoethane u 0.000648 0.00250 1 01/14/202117:40 WG1605648 Dibromomethane U 0.000750 0.00500 1 01/14/202117:40 WG1605648 1,2-Dichlorobenzene u 0.000425 0.00500 1 01/14/202117:40 WG1605648 1,3-Dichlorobenzene u 0.000600 0.00500 1 01/14/202117:40 WG1605648 1,4-Dichlorobenzene u 0.000700 0.00500 1 01/14/202117:40 WG1605648 Dichlorodifluoromethane U 0.00161 0.00250 1 01/14/2021 17:40 WG1605648 1,1-Dichloroethane u 0.000491 0.00250 1 01/14/202117:40 WG1605648 1,2-Dichloroethane U 0.000649 0.00250 1 01/14/202117:40 WG1605648 1,1-Dichloroethene u 0.000606 0.00250 1 01/14/202117:40 WG1605648 cis-1,2-Dichloroethene U 0.000734 0.00250 1 01/14/202117:40 WG1605648 trans-1,2-Dichloroethene u 0.00104 0.00500 1 01/14/202117:40 WG1605648 1,2-Dichloropropane U 0.00142 0.00500 1 01/14/202117:40 WG1605648 1,1-Dichloropropene u 0.000809 0.00250 1 01/14/202117:40 WG1605648 1,3-Dichloropropane u 0.000501 0.00500 1 01/14/202117:40 WG1605648 cis-1,3-Dichloropropene u 0.000757 0.00250 1 01/14/202117:40 WG1605648 trans-1,3-Dichloropropene U 0.00114 0.00500 1 01/14/202117:40 WG1605648 2,2-Dichloropropane u 0.00138 0.00250 1 01/14/202117:40 WG1605648 Di-isopropyl ether U 0.000410 0.00100 1 01/14/202117:40 WG1605648 Ethylbenzene 3.10 0.0295 0.100 40 01/18/2021 01:03 WG1606951 Hexachloro-1,3-butadiene U 0.00600 0.0250 1 01/14/202117:40 WG1605648 lsopropylbenzene 1.34 0.000425 0.00250 1 01/14/202117:40 WG1605648 p-Isopropyltoluene 1.76 0.00255 0.00500 1 01/14/202117:40 WG1605648 2-Buta none (MEK) u 0.0635 0.100 1 01/14/202117:40 WG1605648 Methylene Chloride U 0.00664 0.0250 1 01/14/202117:40 WG1605648 4-Methyl-2-pentanone (MIBK) U 0.00228 0.0250 1 01/14/202117:40 WG1605648 Methyl tert-butyl ether U 0.000350 0.00100 1 01/ 4/2021 17:40 WG1605648 Naphthalene 0.0697 J4 0.00488 0.0125 1 01/14/202117:40 WG1605648 n-Propylbenzene 3.04 0.0380 0.200 40 01/18/202101:03 WG1606951 Styrene u 0.000229 0.0125 1 01/14/202117:40 WG1605648 1,1,1,2-Tetrachloroethane U 0.000948 0.00250 1 01/1 4/2021 17:40 WG1605648 1,1,2,2-Tetrachloroethane U 0.000695 0.00250 1 01/14/202117:40 WG1605648 1,1,2-Trichlorotrifluoroethane U 0.000754 0.00250 1 01/14/202117:40 WG1605648 Tetrachloroethene U 0.000896 0.00250 1 01/14/202117:40 WG1605648 Toluene 2.16 0.00130 0.00500 1 01/14/202117:40 WG1605648 1,2,3-Trichlorobenzene U 0.00733 0.0125 1 01/14/202117:40 WG1605648 1,2,4-Trichlorobenzene U 0.00440 0.0125 1 01/14/202117:40 WG1605648 1,1,1-Trichloroethane U 0.000923 0.00250 1 01/14/202117:40 WG1605648 1,1,2-Trichloroethane U 0.000597 0.00250 1 01/14/202117:40 WG1605648 Trichloroethene U 0.000584 0.00100 1 01/14/202117:40 WG1605648 Trichlorofluoromethane U 0.000827 0.00250 1 01/14/2021 17:40 WG1605648 1,2,3-Trichloropropane u 0.00162 0.0125 1 01/14/202117:40 WG1605648 1,2,4-Trimethylbenzene 18.9 0.0632 0.200 40 01/18/202101:03 WG1606951 1,2,3-Trimethylbenzene 9.01 0.0632 0.200 40 01/18/2021 01:03 WG1606951 1,3,5-Trimethylbenzene 4.39 0.0800 0.200 40 01/18/2021 01:03 WG1606951 Vinyl chloride U 0.00116 0.00250 1 01/14/202117:40 WG1605648 Xylenes, Total 16.5 0.0352 0.260 40 01/18/2021 01:03 WG1606951 (5) Toluene-d8 136 J1 75.0-131 01/14/202117:40 VVG1605648 (S) Toluene-d8 978 75.0-131 01/18/202101:03 WG1606951 (S) 4-Bromotluoro benzene 308 J1 670-138 004/202117:40 W61605648 (S)4-Bromofluorobenzene 115 670-138 01/18/202101:03 WG1606951 (S) 42-Dichloroethane-d4 85.8 70.0-130 01/14/202117:40 WG1605648 (5)1,2-Dichloroethone-d4 97.2 70.0-130 01/18/202101:03 WG1606951 Sample Narrative: Cn 5 Sr Al Sc WR3341 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. * Collected date/time: 01/07/21 00:00 L1305410 Volatile Organic Compounds (GC/MS) by Method 8260B L1305410-01 WG1605648: Surrogate failure due to matrix interference. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR - Patriot Environmental Services 11-21-00012 L1305410 01/19/21 09:43 6 of 23