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L1396822-23 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) <br />(OS) L1396822-23 <br />Analyte <br />09/02/21 17:5 2 • (MS) R3699951-5 09/02/2118:01 <br />Spike Amount Original Result MS Result <br />mg/kg mg/kg mg/kg <br />(MSD) R3699951-6 09/02/2118:04 <br />MSD Result MS Rec. <br />mg/kg <br />MSD Rec. <br />54.1 <br />Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits <br />Antimony 100 U 55.9 54.1 55.9 1 75.0-125 J6 J6 3.18 20 <br />Arsenic 100 2.06 98.0 96.0 95.9 93.9 1 75.0-125 2.08 20 <br />Barium 100 150 305 389 155 239 1 75.0-125 J5 J3 J5 24.2 20 <br />Beryllium 100 0.611 98.3 95.1 97.7 94.5 1 75.0-125 3.29 20 <br />Cadmium 100 0.175 97.2 94.0 97.1 93.8 1 75.0-125 3.37 20 <br />Chromium 100 21.4 108 107 86.8 85.4 1 75.0-125 1.31 20 <br />Cobalt 100 7.43 111 109 104 102 1 75.0-125 1.91 20 <br />Copper 100 17.7 119 115 101 97.1 1 75.0-125 3.49 20 <br />Lead 100 49.0 162 159 113 111 1 75.0-125 1.42 20 <br />Molybdenum 100 u 95.3 91.2 95.3 91.2 1 75.0-125 4.31 20 <br />Nickel 100 23.8 113 111 89.2 87.7 1 75.0-125 1.39 20 <br />Selenium 100 u 97.9 94.6 97.9 94.6 1 75.0-125 3.40 20 <br />Silver 20.0 u 18.3 18.0 91.7 90.1 1 75.0-125 1.73 20 <br />Thallium 100 u 95.5 92.1 95.5 92.1 1 75.0-125 3.69 20 <br />Vanadium 100 23.6 118 123 94.9 99.4 1 75.0-125 3.80 20 <br />Zinc 100 52.8 147 157 94.0 104 1 75.0-125 6.39 20 <br />WG1733192 QUALITY CONTROL SUMMARY <br />Metals (ICP) by Method 60108 L1396533-01,02,03 <br />5 <br />Sr <br />4 <br />Cn <br />3 <br />Ss <br />Cp <br />2 <br />Tc <br />Sc <br />7 <br />GI <br />Al <br />ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br />Patriot Environmental - McClellan, CA 11.21.00450 L1396533 09/08/21 09:43 20 of 42