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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11414-002-SA Date Extracted: 04-13-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-17-2018
<br />Client ID: VS3 Date Received: 04-02-2018 GC Column: DB5MS 2005 WHO TEQ: 0.00529
<br />Matrix: Soil Amount: 5.07 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4472 % Solids: 96.41
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.0914 - 0.0315
<br />1,2,3,7,8-PeCDD ND 0.201 -0.0468
<br />1,2,3,4,7,8-HxCDD ND 0.343 -0.0503
<br />1,2,3,6,7,8-HxCDD ND 0.371 -0.0490 Total TCDD ND 0.0914
<br />1,2,3,7,8,9-HxCDD ND 0.347 -0.0488 Total PeCDD ND 0.201
<br />1,2,3,4,6,7,8-HpCDD 0.460 - J 0.00460 0.0541 Total HxCDD ND 0.371
<br />OCDD 2.30 - J 0.000690 0.0888 Total HpCDD 1.12 -J
<br />2,3,7,8-TCDF ND 0.104 -0.0243
<br />1,2,3,7,8-PeCDF ND 0.150 -0.0285
<br />2,3,4,7,8-PeCDF ND 0.144 -0.0298
<br />1,2,3,4,7,8-HxCDF ND 0.103 -0.0255
<br />1,2,3,6,7,8-HxCDF ND 0.101 - 0.0253
<br />2,3,4,6,7,8-HxCDF ND 0.115 - 0.0279
<br />1,2,3,7,8,9-HxCDF ND 0.142 -0.0367 Total TCDF ND 0.104
<br />1,2,3,4,6,7,8-HpCDF ND 0.159 -0.0321 Total PeCDF ND 0.150
<br />1,2,3,4,7,8,9-HpCDF ND 0.201 -0.0396 Total HxCDF ND 0.142
<br />OCDF ND 0.355 -0.0843 Total HpCDF ND 0.201
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 95.7 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 83.1 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 84.4 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 89.6 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 86.9 23.0 - 140
<br />13C-OCDD 64.6 17.0 - 157
<br />13C-2,3,7,8-TCDF 102 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 74.9 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 78.4 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 99.7 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 103 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 95.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 94.4 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 78.3 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 83.0 26.0 - 138
<br />13C-OCDF 68.2 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 97.1 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/17/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/17/2018
<br />of 000011000006
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