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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11414-004-SA Date Extracted: 04-13-2018 ICal: PCDDFAL3-12-22-17 Acquired: 04-17-2018
<br />Client ID: VS7 Date Received: 04-02-2018 GC Column: DB5MS 2005 WHO TEQ: 0.665
<br />Matrix: Soil Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4472 % Solids: 96.52
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.138 - 0.0315
<br />1,2,3,7,8-PeCDD ND 0.331 -0.0468
<br />1,2,3,4,7,8-HxCDD ND 0.290 -0.0503
<br />1,2,3,6,7,8-HxCDD 0.714 - J 0.0714 0.0490 Total TCDD ND 0.138
<br />1,2,3,7,8,9-HxCDD 0.526 - J 0.0526 0.0488 Total PeCDD ND 0.331
<br />1,2,3,4,6,7,8-HpCDD 10.4 -0.104 0.0541 Total HxCDD 5.34 -
<br />OCDD 67.9 -0.0204 0.0888 Total HpCDD 19.1 -
<br />2,3,7,8-TCDF 0.523 - J 0.0523 0.0243
<br />1,2,3,7,8-PeCDF ND 0.204 -0.0285
<br />2,3,4,7,8-PeCDF 0.637 - J 0.191 0.0298
<br />1,2,3,4,7,8-HxCDF 0.571 - J 0.0571 0.0255
<br />1,2,3,6,7,8-HxCDF 0.407 - J 0.0407 0.0253
<br />2,3,4,6,7,8-HxCDF 0.366 - J 0.0366 0.0279
<br />1,2,3,7,8,9-HxCDF ND 0.218 -0.0367 Total TCDF 3.35 -
<br />1,2,3,4,6,7,8-HpCDF 3.64 - J 0.0364 0.0321 Total PeCDF 7.46 -
<br />1,2,3,4,7,8,9-HpCDF ND 0.377 -0.0396 Total HxCDF 6.54 -
<br />OCDF 7.64 - J 0.00229 0.0843 Total HpCDF 8.50 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 104 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 89.6 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 85.1 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 94.7 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 101 23.0 - 140
<br />13C-OCDD 86.2 17.0 - 157
<br />13C-2,3,7,8-TCDF 104 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 80.7 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 82.7 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 103 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 107 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 105 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 105 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 86.9 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 97.9 26.0 - 138
<br />13C-OCDF 85.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 98.5 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/17/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />4/17/2018
<br />of 000011000008
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