|
EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-001-MB Date Extracted: 04-16-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: Method Blank Date Received: NA GC Column: DB5MS 2005 WHO TEQ: 0.0
<br />Matrix: Solid Amount: 5.00 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4473
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.271 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.342 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.395 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.463 -0.0940 Total TCDD ND 0.271
<br />1,2,3,7,8,9-HxCDD ND 0.393 -0.0823 Total PeCDD ND 0.342
<br />1,2,3,4,6,7,8-HpCDD ND 0.544 -0.0842 Total HxCDD ND 0.463
<br />OCDD ND 0.711 - 0.172 Total HpCDD ND 0.544
<br />2,3,7,8-TCDF ND 0.200 -0.0269
<br />1,2,3,7,8-PeCDF ND 0.222 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.233 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.251 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.253 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.281 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.320 -0.0657 Total TCDF ND 0.200
<br />1,2,3,4,6,7,8-HpCDF ND 0.339 -0.0747 Total PeCDF ND 0.233
<br />1,2,3,4,7,8,9-HpCDF ND 0.430 -0.0883 Total HxCDF ND 0.320
<br />OCDF ND 0.606 -0.170 Total HpCDF ND 0.430
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 80.2 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 82.2 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 82.5 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 84.6 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 78.2 23.0 - 140
<br />13C-OCDD 65.4 17.0 - 157
<br />13C-2,3,7,8-TCDF 83.0 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 78.9 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 78.9 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 80.4 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 79.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 75.3 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 73.8 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 75.9 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 77.0 26.0 - 138
<br />13C-OCDF 67.4 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 76.9 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/18/2018 4/18/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />000003 of 000033
|