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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-015-SA Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-18-2018
<br />Client ID: SP1-15 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 3.20
<br />Matrix: Solid Amount: 5.02 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475 % Solids: 94.28
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.179 - 0.0273
<br />1,2,3,7,8-PeCDD 0.753 - J 0.753 0.0570
<br />1,2,3,4,7,8-HxCDD 0.897 - J 0.0897 0.0793
<br />1,2,3,6,7,8-HxCDD 2.91 - J 0.291 0.0940 Total TCDD 0.467 -J
<br />1,2,3,7,8,9-HxCDD 1.93 - J 0.193 0.0823 Total PeCDD 4.35 -J
<br />1,2,3,4,6,7,8-HpCDD 67.2 -0.672 0.0842 Total HxCDD 22.6 -
<br />OCDD 546 -0.164 0.172 Total HpCDD 122 -
<br />2,3,7,8-TCDF 1.78 -0.178 0.0269
<br />1,2,3,7,8-PeCDF 0.368 - J 0.0110 0.0449
<br />2,3,4,7,8-PeCDF 1.11 - J 0.333 0.0468
<br />1,2,3,4,7,8-HxCDF 1.25 - J 0.125 0.0437
<br />1,2,3,6,7,8-HxCDF 0.872 - J 0.0872 0.0417
<br />2,3,4,6,7,8-HxCDF 1.02 - J 0.102 0.0574
<br />1,2,3,7,8,9-HxCDF 0.450 - J 0.0450 0.0657 Total TCDF 10.7 -
<br />1,2,3,4,6,7,8-HpCDF 14.0 -0.140 0.0747 Total PeCDF 11.1 -
<br />1,2,3,4,7,8,9-HpCDF 0.992 - J 0.00992 0.0883 Total HxCDF 19.9 -
<br />OCDF 33.5 -0.0101 0.170 Total HpCDF 37.6 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 94.1 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 96.9 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 99.7 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 96.8 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 87.6 23.0 - 140
<br />13C-OCDD 75.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 97.3 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 94.6 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 96.1 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 91.5 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 88.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 86.4 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 86.2 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 87.6 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 88.5 26.0 - 138
<br />13C-OCDF 76.9 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 92.6 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
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