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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11423-020-SA Date Extracted: 04-17-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-19-2018
<br />Client ID: SP1-20 Date Received: 04-04-2018 GC Column: DB5MS 2005 WHO TEQ: 3.62
<br />Matrix: Solid Amount: 5.03 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4475 % Solids: 93.51
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.210 - 0.0273
<br />1,2,3,7,8-PeCDD 0.856 - J 0.856 0.0570
<br />1,2,3,4,7,8-HxCDD 1.19 - J 0.119 0.0793
<br />1,2,3,6,7,8-HxCDD 3.04 - J 0.304 0.0940 Total TCDD 0.546 -J
<br />1,2,3,7,8,9-HxCDD 2.00 - J 0.200 0.0823 Total PeCDD 4.16 -J
<br />1,2,3,4,6,7,8-HpCDD 55.7 -0.557 0.0842 Total HxCDD 20.1 -
<br />OCDD 455 -0.137 0.172 Total HpCDD 100 -
<br />2,3,7,8-TCDF 2.58 - F 0.258 0.0269
<br />1,2,3,7,8-PeCDF 0.736 - J 0.0221 0.0449
<br />2,3,4,7,8-PeCDF 1.66 - J 0.498 0.0468
<br />1,2,3,4,7,8-HxCDF 1.88 - J 0.188 0.0437
<br />1,2,3,6,7,8-HxCDF 1.12 - J 0.112 0.0417
<br />2,3,4,6,7,8-HxCDF 1.45 - J 0.145 0.0574
<br />1,2,3,7,8,9-HxCDF 0.856 - J 0.0856 0.0657 Total TCDF 14.6 -
<br />1,2,3,4,6,7,8-HpCDF 11.3 -0.113 0.0747 Total PeCDF 13.2 -
<br />1,2,3,4,7,8,9-HpCDF 1.60 - J 0.0160 0.0883 Total HxCDF 18.4 -
<br />OCDF 27.4 -0.00822 0.170 Total HpCDF 32.2 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 97.5 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 101 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 104 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 99.2 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 93.2 23.0 - 140
<br />13C-OCDD 76.8 17.0 - 157
<br />13C-2,3,7,8-TCDF 102 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 96.9 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 98.5 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 93.1 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 91.3 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 89.2 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 89.7 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 91.0 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 93.5 26.0 - 138
<br />13C-OCDF 81.8 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 89.8 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/19/2018 4/19/2018
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