|
EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11441-002-SA Date Extracted: 04-26-2018 ICal: PCDDFAL4-12-20-17 Acquired: 04-28-2018
<br />Client ID: VS20 Date Received: 04-11-2018 GC Column: DB5MS 2005 WHO TEQ: 0.252
<br />Matrix: Soil Amount: 5.01 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4491 % Solids: 90.84
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.216 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.269 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.226 -0.0793
<br />1,2,3,6,7,8-HxCDD 0.844 - J 0.0844 0.0940 Total TCDD 0.855 -J
<br />1,2,3,7,8,9-HxCDD ND 0.216 -0.0823 Total PeCDD ND 0.269
<br />1,2,3,4,6,7,8-HpCDD 4.16 - J 0.0416 0.0842 Total HxCDD 3.76 -J
<br />OCDD 19.3 -0.00579 0.172 Total HpCDD 8.35 -
<br />2,3,7,8-TCDF ND 0.170 -0.0269
<br />1,2,3,7,8-PeCDF ND 0.184 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.196 -0.0468
<br />1,2,3,4,7,8-HxCDF 0.339 - J 0.0339 0.0437
<br />1,2,3,6,7,8-HxCDF 0.595 - J 0.0595 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.148 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.156 -0.0657 Total TCDF 1.39 -
<br />1,2,3,4,6,7,8-HpCDF 2.52 - J 0.0252 0.0747 Total PeCDF 3.58 -D,J,M
<br />1,2,3,4,7,8,9-HpCDF ND 0.247 -0.0883 Total HxCDF 10.3 -D,M
<br />OCDF 4.00 - J 0.00120 0.170 Total HpCDF 9.04 -
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 81.6 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 86.0 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 87.4 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 87.5 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 80.3 23.0 - 140
<br />13C-OCDD 68.9 17.0 - 157
<br />13C-2,3,7,8-TCDF 84.3 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 82.0 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 83.2 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 84.5 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 81.1 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 78.6 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 78.9 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 79.2 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 79.6 26.0 - 138
<br />13C-OCDF 69.0 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 78.9 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />4/30/2018 4/30/2018
<br />5172 Hillsdale Circle * El Dorado Hills, CA 95762 * Tel (916) 934-0900 * Fax (916) 934-0999 * www.frontieranalytical.com
<br />of 000016000006
|