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EPA Method 1613
<br />PCDD/F
<br />FAL ID: 11471-001-MB Date Extracted: 04-30-2018 ICal: PCDDFAL4-12-20-17 Acquired: 05-01-2018
<br />Client ID: Method Blank Date Received: NA GC Column: DB5MS 2005 WHO TEQ: 0.0
<br />Matrix: Soil Amount: 5.00 g Units: pg/g Basis: Dry Weight
<br />Batch No: X4493
<br />Compound Conc DL Qual
<br />2005
<br />WHO Tox MDL Compound Conc DL Qual
<br />2,3,7,8-TCDD ND 0.151 - 0.0273
<br />1,2,3,7,8-PeCDD ND 0.182 -0.0570
<br />1,2,3,4,7,8-HxCDD ND 0.197 -0.0793
<br />1,2,3,6,7,8-HxCDD ND 0.221 -0.0940 Total TCDD ND 0.151
<br />1,2,3,7,8,9-HxCDD ND 0.191 -0.0823 Total PeCDD ND 0.182
<br />1,2,3,4,6,7,8-HpCDD ND 0.180 -0.0842 Total HxCDD ND 0.221
<br />OCDD ND 0.314 - 0.172 Total HpCDD ND 0.180
<br />2,3,7,8-TCDF ND 0.116 -0.0269
<br />1,2,3,7,8-PeCDF ND 0.140 -0.0449
<br />2,3,4,7,8-PeCDF ND 0.141 -0.0468
<br />1,2,3,4,7,8-HxCDF ND 0.126 -0.0437
<br />1,2,3,6,7,8-HxCDF ND 0.137 - 0.0417
<br />2,3,4,6,7,8-HxCDF ND 0.132 - 0.0574
<br />1,2,3,7,8,9-HxCDF ND 0.160 -0.0657 Total TCDF ND 0.116
<br />1,2,3,4,6,7,8-HpCDF ND 0.122 -0.0747 Total PeCDF ND 0.141
<br />1,2,3,4,7,8,9-HpCDF ND 0.211 -0.0883 Total HxCDF ND 0.160
<br />OCDF ND 0.225 -0.170 Total HpCDF ND 0.211
<br />Internal Standards % Rec QC Limits Qual
<br />13C-2,3,7,8-TCDD 104 25.0 - 164
<br />13C-1,2,3,7,8-PeCDD 107 25.0 - 181
<br />13C-1,2,3,4,7,8-HxCDD 110 32.0 - 141
<br />13C-1,2,3,6,7,8-HxCDD 107 28.0 - 130
<br />13C-1,2,3,4,6,7,8-HpCDD 105 23.0 - 140
<br />13C-OCDD 101 17.0 - 157
<br />13C-2,3,7,8-TCDF 111 24.0 - 169
<br />13C-1,2,3,7,8-PeCDF 104 24.0 - 185
<br />13C-2,3,4,7,8-PeCDF 108 21.0 - 178
<br />13C-1,2,3,4,7,8-HxCDF 99.4 26.0 - 152
<br />13C-1,2,3,6,7,8-HxCDF 98.5 26.0 - 123
<br />13C-2,3,4,6,7,8-HxCDF 99.1 28.0 - 136
<br />13C-1,2,3,7,8,9-HxCDF 97.8 29.0 - 147
<br />13C-1,2,3,4,6,7,8-HpCDF 98.8 28.0 - 143
<br />13C-1,2,3,4,7,8,9-HpCDF 75.9 26.0 - 138
<br />13C-OCDF 97.2 17.0 - 157
<br />Cleanup Surrogate
<br />37Cl-2,3,7,8-TCDD 94.0 35.0 - 197
<br />Analyst:Reviewed By:
<br />Date:Date:
<br />A Isotopic Labeled Standard outside QC range but
<br />signal to noise ratio is >10:1
<br />B Analyte is present in Method Blank
<br />C Chemical Interference
<br />D Presence of Diphenyl Ethers
<br />DNQ Analyte concentration is below calibration range
<br />E Analyte concentration is above calibration range
<br />F Analyte confirmation on secondary column
<br />J Analyte concentration is below calibration range
<br />M Maximum possible concentration
<br />ND Analyte Not Detected at Detection Limit Level
<br />NP Not Provided
<br />P Pre-filtered through a Whatman 0.7um GF/F filter
<br />S Sample acceptance criteria not met
<br />X Matrix interferences
<br />* Result taken from dilution or reinjection
<br />5/2/2018 5/2/2018
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