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DRUMS OILY SLUDGE #2 SAMPLE RESULTS - 02 Collected date/time: 08/11/21 07:00 L1391519 Volatile Organic Compounds (GC/MS) by Method 82608 Result Qualifier MDL RDL Dilution Analysis Batch Cp Analyte mg/kg mg/kg mg/kg date/time Bromodichloromethane U 0.00290 0.0100 4 08/23/202115:54 WG1727785 FTc Bromoform U 0.00468 0.100 4 08/23/202115:54 WG1727785 Bromomethane U 0.00788 0.0500 4 08/23/202115:54 WG1727785 FSS n-Butylbenzene U 0.0210 0.0500 4 08/23/202115:54 WG1727785 sec-Butyl benzene 0.0147 J 0.0115 0.0500 4 08/23/202115:54 WG1727785 tert-Butylbenzene U 0.00780 0.0200 4 08/23/202115:54 WG1727785 4 Cn Carbon tetrachloride U 0.00359 0.0200 4 08/23/202115:54 WG1727785 Chlorobenzene U 0.000840 0.0100 4 08/23/202115:54 WG1727785 Chlorodibromomethane U 0.00245 0.0100 4 08/23/202115:54 WG1727785 Chloroethane U 0.00680 0.0200 4 08/23/202115:54 WG1727785 Chloroform U 0.00412 0.0100 4 08/23/202115:54 WG1727785 RC Chloromethane U 0.0174 0.0500 4 08/23/202115:54 WG1727785 2-Chlorotoluene U 0.00346 0.0100 4 08/23/202115:54 WG1727785 4-Chlorotoluene U 0.00180 0.0200 4 08/23/202115:54 WG1727785 ql 1,2-Dibromo-3-Chloropropane U 0.0156 0.100 4 08/23/202115:54 WG1727785 1,2-Dibromoethane U 0.00259 0.0100 4 08/23/202115:54 WG1727785 FAI Dibromomethane U 0.00300 0.0200 4 08/23/202115:54 WG1727785 1,2-Dichlorobenzene U 0.00170 0.0200 4 08/23/202115:54 WG1727785 FSC 1,3-Dichlorobenzene U 0.00240 0.0200 4 08/23/202115:54 WG1727785 1,4-Dichlorobenzene U 0.00280 0.0200 4 08/23/202115:54 WG1727785 Dichlorodifluoromethane U 0.00644 0.0100 4 08/23/202115:54 WG1727785 1,1-Dichloroethane U 0.00196 0.0100 4 08/23/202115:54 WG1727785 1,2-Dichloroethane U 0.00260 0.0100 4 08/23/202115:54 WG1727785 1,1-Dichloroethene U 0.00242 0.0100 4 08/23/202115:54 WG1727785 cis-1,2-Dichloroethene U 0.00294 0.0100 4 08/23/202115:54 WG1727785 trans-1,2-Dichloroethene U 0.00416 0.0200 4 08/23/202115:54 WG1727785 1,2-Dichloropropane U 0.00568 0.0200 4 08/23/202115:54 WG1727785 1,1-Dichloropropene U 0.00324 0.0100 4 08/23/202115:54 WG1727785 1,3-Dichloropropane U 0.00200 0.0200 4 08/23/202115:54 WG1727785 cis-1,3-Dichloropropene U 0.00303 0.0100 4 08/23/202115:54 WG1727785 trans-1,3-Dichloropropene U 0.00456 0.0200 4 08/23/202115:54 WG1727785 2,2-Dichloropropane U 0.00552 0.0100 4 08/23/202115:54 WG1727785 Di-isopropyl ether U 0.00164 0.00400 4 08/23/202115:54 WG1727785 Ethylbenzene 0.00420 J 0.00295 0.0100 4 08/23/202115:54 WG1727785 Hexachloro-1,3-butadiene U 0.0240 0.100 4 08/23/202115:54 WG1727785 Isopropylbenzene 0.00370 J 0.00170 0.0100 4 08/23/202115:54 WG1727785 p-Isopropyltoluene 0.0175 J 0.0102 0.0200 4 08/23/202115:54 WG1727785 2-Butanone(MEK) U J4 0.254 0.400 4 08/23/202115:54 WG1727785 Methylene Chloride U 0.0266 0.100 4 08/23/202115:54 WG1727785 4-Methyl-2-pentanone(MIBK) 0.0191 J 0.00912 0.100 4 08/23/202115:54 WG1727785 Methyl tert-butyl ether U 0.00140 0.00400 4 08/23/202115:54 WG1727785 Naphthalene 0.0629 0.0195 0.0500 4 08/23/202115:54 WG1727785 n-Propylbenzene 0.0123 J 0.00380 0.0200 4 08/23/202115:54 WG1727785 Styrene U 0.000916 0.0500 4 08/23/202115:54 WG1727785 1,1,1,2-Tetrachloroethane U 0.00379 0.0100 4 08/23/202115:54 WG1727785 1,1,2,2-Tetrachloroethane U 0.00278 0.0100 4 08/23/202115:54 WG1727785 1,1,2-Trichlorotrifluoroethane U 0.00302 0.0100 4 08/23/202115:54 WG1727785 Tetrachloroethene U 0.00358 0.0100 4 08/23/202115:54 WG1727785 Toluene U 0.00520 0.0200 4 08/23/202115:54 WG1727785 1,2,3-Trichlorobenzene U 0.0293 0.0500 4 08/23/202115:54 WG1727785 1,2,4-Trichlorobenzene U 0.0176 0.0500 4 08/23/202115:54 WG1727785 1,1,1-Trichloroethane U 0.00369 0.0100 4 08/23/202115:54 WG1727785 1,1,2-Trichloroethane U 0.00239 0.0100 4 08/23/202115:54 WG1727785 Trichloroethene U 0.00234 0.00400 4 08/23/202115:54 WG1727785 Trichlorofluoromethane U 0.00331 0.0100 4 08/23/202115:54 WG1727785 1,2,3-Trichloropropane U 0.00648 0.0500 4 08/23/202115:54 WG1727785 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS 81046-16 L1391519 08/27/2109:46 10 of 44