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WG1727785 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 82606 L1391519-02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3695410-1 08/23/2110:04•(LCSD)R3695410-2 08/23/2110:23 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/kg mg/kg mg/kg % % % % % TC Naphthalene 0.125 0.114 0.122 91.2 97.6 59.0-130 6.78 20 n-Propylbenzene 0.125 0.140 0.139 112 111 74.0-126 0.717 20 FSS Styrene 0.125 0.115 0.114 92.0 91.2 72.0-127 0.873 20 1,1,1,2-Tetrachloroethane 0.125 0.119 0.115 95.2 92.0 74.0-129 3.42 20 rCn 1,1,2,2-Tetrachloroethane 0.125 0.151 0.150 121 120 68.0-128 0.664 20 Tetrachloroethene 0.125 0.119 0.121 95.2 96.8 70.0-136 1.67 20 Toluene 0.125 0.128 0.129 102 103 75.0-121 0.778 20 FSr 1,1,2-Trichlorotrifluoroethane 0.125 0.104 0.107 83.2 85.6 61.0-139 2.84 20 1,2,3-Trichlorobenzene 0.125 0.0935 0.107 74.8 85.6 59.0-139 13.5 20 1,2,4-Trichlorobenzene 0.125 0.123 0.130 98.4 104 62.0-137 5.53 20 1,1,1-Trichloroethane 0.125 0.117 0.116 93.6 92.8 69.0-126 0.858 20 1,1,2-Trichloroethane 0.125 0.133 0.134 106 107 78.0-123 0.749 20 7G1 Trichloroethene 0.125 0.123 0.122 98.4 97.6 76.0-126 0.816 20 Trichlorofluoromethane 0.125 0.108 0.108 86.4 86.4 61.0-142 0.000 20 1,2,3-Trichloropropane 0.125 0.136 0.137 109 110 67.0-129 0.733 20 FAI 1,2,3-Trim ethyl benzene 0.125 0.129 0.131 103 105 74.0-124 1.54 20 1,2,4-Trimethylbenzene 0.125 0.126 0.127 101 102 70.0-126 0.791 20 FSC 1,3,5-Trim ethyl benzene 0.125 0.129 0.128 103 102 73.0-127 0.778 20 Vinyl chloride 0.125 0.126 0.133 101 106 63.0-134 5.41 20 Xylenes,Total 0.375 0.364 0.362 97.1 96.5 72.0-127 0.551 20 (S)Toluene-d8 103 103 75.0-131 (S)4-Bromofluorobenzene 90.6 90.8 67.0-138 (S)1,2-Dich/oroethane-d4 103 103 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS 81046-16 L1391519 08/27/2109:46 35 of 44