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DRUMS OILY SLUDGE #5 SAMPLE RESULTS - 05 <br /> Collected date/time: 10/11/21 13:55 L1416813 <br /> Volatile Organic Compounds (GC/MS) by Method 82606 <br /> Result(dry) Qualifier MDL(dry) RDL(dry) Dilution Analysis Batch Cp <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> 1,2,4-Trimethyl benzene 7.77 0.0588 0.186 8.08 10/22/202112:42 WG1761765 FTc <br /> 1,2,3-Trimethyl benzene 4.92 0.0588 0.186 8.08 10/22/202112:42 WG1761765 <br /> 1,3,5-Trimethyl benzene 1.79 0.0745 0.186 8.08 10/22/202112:42 WG1761765 FSS <br /> Vinyl chloride U 0.0431 0.0928 8.08 10/22/202112:42 WG1761765 <br /> Xylenes,Total 1.36 0.0327 0.241 8.08 10/22/202112:42 WG1761765 <br /> (S)Toluene-d8 101 75.0-131 10/22/202112.42 WG1761765 4Cn <br /> (S)4-Bromofluorobenzene 107 67.0-138 10/22/202112.42 WG1761765 <br /> (S)1,2-Dich/oroethone-d4 95.1 70.0-130 10/22/202112.42 WG1761765 <br /> Semi-Volatile Organic Compounds (GC) by Method 8015 <br /> Result(dry) Qualifier MDL(dry) RDL(dry) Dilution Analysis Batch RCAnalyte mg/kg mg/kg mg/kg date/time <br /> C12-C22 Hydrocarbons 202000 12400 67500 6000 10/20/202110:24 WG1759991 GI <br /> C22-C32 Hydrocarbons 486000 22400 67500 6000 10/20/202110:24 WG1759991 <br /> C32-C40 Hydrocarbons 624000 22400 67500 6000 10/20/202110:24 WG1759991 rAl(S)o-Terpheny/ 0.000 J7 18.0-148 10/20/202110:24 WG1759991 <br /> Semi Volatile Organic Compounds (GC/MS) by Method 8270C [ScResult(dry) Qualifier MDL(dry) RDL(dry) Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> Acenaphthene U 90.8 562 6000 10/22/202114:46 WG1760376 <br /> Acenaphthylene U 79.0 562 6000 10/22/202114:46 WG1760376 <br /> Anthracene U 100 562 6000 10/22/202114:46 WG1760376 <br /> Benzidine U 1060 28100 6000 10/22/202114:46 WG1760376 <br /> Benzo(a)anthracene U 98.9 562 6000 10/22/202114:46 WG1760376 <br /> Benzo(b)fluoranthene U 105 562 6000 10/22/202114:46 WG1760376 <br /> Benzo(k)fluoranthene U 99.8 562 6000 10/22/202114:46 WG1760376 <br /> Benzo(g,h,i)perylene U 103 562 6000 10/22/202114:46 WG1760376 <br /> Benzo(a)pyrene U 104 562 6000 10/22/202114:46 WG1760376 <br /> Bis(2-chlorethoxy)methane U 169 5620 6000 10/22/202114:46 WG1760376 <br /> Bis(2-chloroethyl)ether U 185 5620 6000 10/22/202114:46 WG1760376 <br /> 2,2-Oxybis(1-Chloropropane) U 243 5620 6000 10/22/202114:46 WG1760376 <br /> 4-Bromophenyl-phenylether U 197 5620 6000 10/22/202114:46 WG1760376 <br /> 2-Chloronaphthalene U 98.7 562 6000 10/22/202114:46 WG1760376 <br /> 4-Chlorophenyl-phenylether U 196 5620 6000 10/22/202114:46 WG1760376 <br /> Chrysene U 112 562 6000 10/22/202114:46 WG1760376 <br /> Dibenz(a,h)anthracene U 156 562 6000 10/22/202114:46 WG1760376 <br /> 3,3-Dichlorobenzidine U 207 5620 6000 10/22/202114:46 WG1760376 <br /> 2,4-Dinitrotoluene U 161 5620 6000 10/22/202114:46 WG1760376 <br /> 2,6-Dinitrotoluene U 184 5620 6000 10/22/202114:46 WG1760376 <br /> Fluoranthene U 101 562 6000 10/22/202114:46 WG1760376 <br /> Fluorene U 91.3 562 6000 10/22/202114:46 WG1760376 <br /> Hexachlorobenzene U 199 5620 6000 10/22/202114:46 WG1760376 <br /> Hexachloro-1,3-butadiene U 189 5620 6000 10/22/202114:46 WG1760376 <br /> Hexachlorocyclopentadiene U 295 5620 6000 10/22/202114:46 WG1760376 <br /> Hexachloroethane U 221 5620 6000 10/22/202114:46 WG1760376 <br /> Indeno(1,2,3-cd)pyrene U 159 562 6000 10/22/202114:46 WG1760376 <br /> Isophorone U 172 5620 6000 10/22/202114:46 WG1760376 <br /> Naphthalene U 141 562 6000 10/22/202114:46 WG1760376 <br /> Nitrobenzene U 196 5620 6000 10/22/202114:46 WG1760376 <br /> n-Nitrosodimethyla mine U 832 5620 6000 10/22/202114:46 WG1760376 <br /> n-Nitrosodiphenyla mine U 424 5620 6000 10/22/202114:46 WG1760376 <br /> n-Nitrosodi-n-propylamine U 187 5620 6000 10/22/202114:46 WG1760376 <br /> Phenanthrene U 112 562 6000 10/22/202114:46 WG1760376 <br /> Benzylbutyl phthalate U 175 5620 6000 10/22/202114:46 WG1760376 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc AIS 81046-16 L1416813 10/27/2111:35 11 of 41 <br />