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DRUMS OILY SLUDGE #6 SAMPLE RESULTS - 06 Collected date/time: 10/11/21 13:37 L1416813 Volatile Organic Compounds (GC/MS) by Method 82606 Result(dry) Qualifier MDL(dry) RDL(dry) Dilution Analysis Batch Cp Analyte mg/kg mg/kg mg/kg date/time Acetone 16.6 1_ 13.8 18.9 8 10/22/202113:01 WG1761765 FTc Acrylonitrile U 1.37 4.72 8 10/22/202113:01 WG1761765 Benzene U 0.177 0.378 8 10/22/202113:01 WG1761765 3 Bromobenzene U 0.340 4.72 8 10/22/202113:01 WG1761765 SS Bromodichloromethane U 0.274 0.945 8 10/22/202113:01 WG1761765 Bromoform U 0.442 9.45 8 10/22/202113:01 WG1761765 4 Cn Bromomethane U 0.746 4.72 8 10/22/202113:01 WG1761765 n-Butylbenzene 24.2 1.98 4.72 8 10/22/202113:01 WG1761765 sec-Butyl benzene 14.6 1.09 4.72 8 10/22/202113:01 WG1761765 tert-Butylbenzene U 0.737 1.89 8 10/22/202113:01 WG1761765 Carbon tetrachloride U 0.339 1.89 8 10/22/202113:01 WG1761765 6 QC Chlorobenzene U 0.0794 0.945 8 10/22/202113:01 WG1761765 Chlorodibromomethane U 0.231 0.945 8 10/22/202113:01 WG1761765 Chloroethane U 0.642 1.89 8 10/22/202113:01 WG1761765 GI Chloroform U 0.389 0.945 8 10/22/202113:01 WG1761765 Chloromethane U 1.64 4.72 8 10/22/202113:01 WG1761765 FAI 2-Chlorotoluene U 0.327 0.945 8 10/22/202113:01 WG1761765 4-Chlorotoluene U 0.170 1.89 8 10/22/202113:01 WG1761765 FSC 1,2-Dibromo-3-Chloropropane U 1.47 9.45 8 10/22/202113:01 WG1761765 1,2-Dibromoethane U 0.245 0.945 8 10/22/202113:01 WG1761765 Dibromomethane U 0.283 1.89 8 10/22/202113:01 WG1761765 1,2-Dichlorobenzene U 0.161 1.89 8 10/22/202113:01 WG1761765 1,3-Dichlorobenzene U 0.227 1.89 8 10/22/202113:01 WG1761765 1,4-Dichlorobenzene U 0.265 1.89 8 10/22/202113:01 WG1761765 Dichlorodifluoromethane U 0.609 0.945 8 10/22/202113:01 WG1761765 1,1-Dichloroethane U 0.186 0.945 8 10/22/202113:01 WG1761765 1,2-Dichloroethane U 0.245 0.945 8 10/22/202113:01 WG1761765 1,1-Dichloroethene U 0.229 0.945 8 10/22/202113:01 WG1761765 cis-1,2-Dichloroethene U 0.277 0.945 8 10/22/202113:01 WG1761765 trans-1,2-Dichloroethene U 0.393 1.89 8 10/22/202113:01 WG1761765 1,2-Dichloropropane U 0.539 1.89 8 10/22/202113:01 WG1761765 1,1-Dichloropropene U 0.306 0.945 8 10/22/202113:01 WG1761765 1,3-Dichloropropane U 0.189 1.89 8 10/22/202113:01 WG1761765 cis-1,3-Dichloropropene U 0.286 0.945 8 10/22/202113:01 WG1761765 trans-1,3-Dichloropropene U 0.431 1.89 8 10/22/202113:01 WG1761765 2,2-Dichloropropane U 0.520 0.945 8 10/22/202113:01 WG1761765 Di-isopropyl ether U 0.155 0.378 8 10/22/202113:01 WG1761765 Ethylbenzene 1.62 0.279 0.945 8 10/22/202113:01 WG1761765 Hexachloro-1,3-butadiene U 2.27 9.45 8 10/22/202113:01 WG1761765 Isopropylbenzene 1.44 0.161 0.945 8 10/22/202113:01 WG1761765 p-Isopropyltoluene 11.4 0.964 1.89 8 10/22/202113:01 WG1761765 2-Butanone(MEK) U 24.0 37.8 8 10/22/202113:01 WG1761765 Methylene Chloride U 2.51 9.45 8 10/22/202113:01 WG1761765 4-Methyl-2-pentanone(MIBK) 0.869 J_ 0.860 9.45 8 10/22/202113:01 WG1761765 Methyl tert-butyl ether U 0.132 0.378 8 10/22/202113:01 WG1761765 Naphthalene 14.8 1.84 4.72 8 10/22/202113:01 WG1761765 n-Propylbenzene 6.42 0.359 1.89 8 10/22/202113:01 WG1761765 Styrene U 0.0864 4.72 8 10/22/202113:01 WG1761765 1,1,1,2-Tetrachloroethane U 0.358 0.945 8 10/22/202113:01 WG1761765 1,1,2,2-Tetrachloroethane U 0.263 0.945 8 10/22/202113:01 WG1761765 1,1,2-Trichlorotrifluoroethane U 0.285 0.945 8 10/22/202113:01 WG1761765 Tetrachloroethene U 0.339 0.945 8 10/22/202113:01 WG1761765 Toluene 3.81 0.491 1.89 8 10/22/202113:01 WG1761765 1,2,3-Trichlorobenzene U 2.77 4.72 8 10/22/202113:01 WG1761765 1,2,4-Trichlorobenzene U 1.66 4.72 8 10/22/202113:01 WG1761765 1,1,1-Trichloroethane U 0.349 0.945 8 10/22/202113:01 WG1761765 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS 81046-16 L1416813 10/27/2111:35 14 of 41