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WG1761765 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 82606 1-1416813-05,06 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) FP1(LCS)R3720147-1 10/22/2109:51•(LCSD)R3720147-2 10/22/2110:10 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec.Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte mg/kg mg/kg mg/kg % % % % % TC Naphthalene 0.125 0.0802 0.0871 64.2 69.7 59.0-130 8.25 20 n-Propylbenzene 0.125 0.125 0.123 100 98.4 74.0-126 1.61 20 FSS Styrene 0.125 0.127 0.127 102 102 72.0-127 0.000 20 1,1,1,2-Tetrachloroethane 0.125 0.120 0.116 96.0 92.8 74.0-129 3.39 20 rCn 1,1,2,2-Tetrachloroethane 0.125 0.103 0.0971 82.4 77.7 68.0-128 5.90 20 Tetrachloroethene 0.125 0.123 0.120 98.4 96.0 70.0-136 2.47 20 Toluene 0.125 0.121 0.118 96.8 94.4 75.0-121 2.51 20 FSr 1,1,2-Trichlorotrifluoroethane 0.125 0.106 0.110 84.8 88.0 61.0-139 3.70 20 1,2,3-Trichlorobenzene 0.125 0.0748 0.0883 59.8 70.6 59.0-139 16.6 20 1,2,4-Trichlorobenzene 0.125 0.0805 0.0872 64.4 69.8 62.0-137 7.99 20 1,1,1-Trichloroethane 0.125 0.125 0.128 100 102 69.0-126 2.37 20 1,1,2-Trichloroethane 0.125 0.118 0.118 94.4 94.4 78.0-123 0.000 20 7G1 Trichloroethene 0.125 0.164 0.166 131 133 76.0-126 J4 J4 1.21 20 Trichlorofluoromethane 0.125 0.119 0.124 95.2 99.2 61.0-142 4.12 20 FAI 1,2,3-Trichloropropane 0.125 0.142 0.135 114 108 67.0-129 5.05 20 1,2,3-Trim ethyl benzene 0.125 0.115 0.117 92.0 93.6 74.0-124 1.72 20 1,2,4-Trimethylbenzene 0.125 0.121 0.120 96.8 96.0 70.0-126 0.830 20 FSC 1,3,5-Trim ethyl benzene 0.125 0.120 0.122 96.0 97.6 73.0-127 1.65 20 Vinyl chloride 0.125 0.123 0.123 98.4 98.4 63.0-134 0.000 20 Xylenes,Total 0.375 0.359 0.355 95.7 94.7 72.0-127 1.12 20 (S)Toluene-d8 104 103 75.0-131 (S)4-Bromofluorobenzene 103 102 670-138 (S)1,2-Dich/oroethane-d4 106 106 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS 81046-16 L1416813 10/27/2111:35 32 of 41