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SAMPLE SUMMARY Collected by Collected date/time Received date/time TRACK SAND/SLUDGE L1426285-01 Solid Juan Rubio 11/01/2109:10 11/03/2114:00 C Method Batch Dilution Preparation Analysis Analyst Location p date/time date/time FTC Total Solids by Method 2540 G-2011 WG1770961 1 11/08/2117:48 11/08/2117:58 VRP Mt.Juliet,TN Mercury by Method 7471A WG1769465 1 11/05/2109:27 11/07/2113:25 MRW Mt.Juliet,TN Metals(ICP)by Method 60108 WG1771409 .1 11/10/2119:28 11/18/2115:46 CCE Mt.Juliet,TN Metals(ICP)by Method 60108 WG1771409 .5 11/10/2119:28 11/19/2111:50 CCE Mt.Juliet,TN Volatile Organic Compounds(GC)by Method 8015 WG1769985 1 11/04/2113:49 11/06/2113:54 BMB Mt.Juliet,TN 4Cr1 Volatile Organic Compounds(GC/MS)by Method 82608 WG1770113 1 11/04/2113:49 11/06/2120:26 ADM Mt.Juliet,TN Semi-Volatile Organic Compounds (GC)by Method 8015 WG1772833 298 11/12/2100:17 11/12/2122:07 JAS Mt.Juliet,TN FSr Collected by Collected date/time Received date/time TRACK SAND/SLUDGE/DEBRIS L1426285-02 Solid Juan Rubio 11/01/2109:22 11/03/2114:00 RC Method Batch Dilution Preparation Analysis Analyst Location date/time date/time GI Mercury by Method 7471A WG1769465 1 11/05/2109:27 11/07/2113:27 MRW Mt.Juliet,TN Metals(ICP)by Method 60108 WG1771409 1 11/10/2119:28 11/18/2115:49 CCE Mt.Juliet,TN FAI Metals(ICP)by Method 60108 WG1771409 5 11/10/2119:28 11/19/2111:52 CCE Mt.Juliet,TN Volatile Organic Compounds(GC)by Method 8015 WG1772179 125 11/04/2113:49 11/10/2117:00 BMB Mt.Juliet,TN FSC Volatile Organic Compounds(GC/MS)by Method 82608 WG1770113 100 11/04/2113:49 11/06/2122:39 ADM Mt.Juliet,TN Semi-Volatile Organic Compounds (GC)by Method 8015 WG1772833 288 11/12/2100:17 11/12/2122:20 JAS Mt.Juliet,TN ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: UPRR-American Integrated Services,Inc AIS Job#81046-50 L1426285 11/19/2116:02 3 of 24