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TRACK SAND/SLUDGE SAMPLE RESULTS - 01 <br /> Collected date/time: 11/01/21 09:10 L1426285 <br /> Total Solids by Method 2540 G-2011 <br /> Result Qualifier Dilution Analysis Batch FP1 <br /> Analyte % date/time <br /> FTCTotal Solids 78.5 1 11/08/202117:58 WG1770961 <br /> Mercury by Method 7471A FSSResult Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time 4Cr1 <br /> Mercury U 0.0180 0.0400 1 11/07/202113:25 WG1769465 <br /> Metals (ICP) by Method 6010B <br /> Result Qualifier MDL RDL Dilution Analysis Batch <br /> 5 <br /> Analyte mg/kg mg/kg mg/kg date/time QC <br /> Antimony 0.133 J 0.0544 0.200 .1 11/18/202115:46 WG1771409 <br /> Arsenic 4.12 0.0518 0.200 .1 11/18/202115:46 WG1771409 AGI <br /> Barium 67.6 0.00852 0.0500 .1 11/18/202115:46 WG1771409 <br /> Beryllium 0.0828 0.00315 0.0200 .1 11/18/202115:46 WG1771409 FAI Cadmium 0.265 0.00471 0.0500 .1 11/18/202115:46 WG1771409 <br /> Chromium 31.1 0.0133 0.100 .1 11/18/202115:46 WG1771409 <br /> Cobalt 6.29 0.0406 0.500 .5 11/19/202111:50 WG1771409 9 <br /> SC <br /> Copper 50.6 0.0400 0.200 .1 11/18/202115:46 WG1771409 <br /> Lead 18.7 0.104 0.250 .5 11/19/202111:50 WG1771409 <br /> Molybdenum 9.46 0.0109 0.0500 .1 11/18/202115:46 WG1771409 <br /> Nickel 38.9 0.0660 1.00 .5 11/19/202111:50 WG1771409 <br /> Selenium U 0.0764 0.200 .1 11/18/202115:46 WG1771409 <br /> Silver 0.0509 J 0.0127 0.100 .1 11/18/202115:46 WG1771409 <br /> Thallium U 0.197 1.00 .5 11/19/202111:50 WG1771409 <br /> Vanadium 12.6 0.0506 0.200 .1 11/18/202115:46 WG1771409 <br /> Zinc 67.7 0.0832 0.500 .1 11/18/202115:46 WG1771409 <br /> Volatile Organic Compounds (GC) by Method 8015 <br /> Result Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> TPHG C5-C12 4.42 0.0332 0.100 1 11/06/202113:54 WG1769985 <br /> (S)a,a,a-Trifluorotoluene(FID) 90.4 T/.0-120 11/06/202113:54 WG1769985 <br /> Volatile Organic Compounds (GC/MS) by Method 8260B <br /> Result Qualifier MDL RDL Dilution Analysis Batch <br /> Analyte mg/kg mg/kg mg/kg date/time <br /> Acetone U J4 0.0365 0.0500 1 11/06/202120:26 WG1770113 <br /> Acrylonitrile U 0.00361 0.0125 1 11/06/202120:26 WG1770113 <br /> Benzene 0.000525 J 0.000467 0.00100 1 11/06/202120:26 WG1770113 <br /> Bromobenzene U 0.000900 0.0125 1 11/06/202120:26 WG1770113 <br /> Bromodichloromethane U 0.000725 0.00250 1 11/06/202120:26 WG1770113 <br /> Bromoform U 0.00117 0.0250 1 11/06/202120:26 WG1770113 <br /> Bromomethane U 0.00197 0.0125 1 11/06/202120:26 WG1770113 <br /> n-Butylbenzene U 0.00525 0.0125 1 11/06/202120:26 WG1770113 <br /> sec-Butyl benzene 0.00768 J 0.00288 0.0125 1 11/06/202120:26 WG1770113 <br /> tet-Butylbenzene U 0.00195 0.00500 1 11/06/202120:26 WG1770113 <br /> Carbon tetrachloride U 0.000898 0.00500 1 11/06/202120:26 WG1770113 <br /> Chlorobenzene U 0.000210 0.00250 1 11/06/202120:26 WG1770113 <br /> Chlorodibromomethane U 0.000612 0.00250 1 11/06/202120:26 WG1770113 <br /> Chloroethane U 0.00170 0.00500 1 11/06/202120:26 WG1770113 <br /> Chloroform U 0.00103 0.00250 1 11/06/202120:26 WG1770113 <br /> Chloromethane U 0.00435 0.0125 1 11/06/202120:26 WG1770113 <br /> 2-Chlorotoluene U 0.000865 0.00250 1 11/06/202120:26 WG1770113 <br /> 4-Chlorotoluene U 0.000450 0.00500 1 11/06/202120:26 WG1770113 <br /> ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: <br /> UPRR-American Integrated Services,Inc AIS Job#81046-50 L1426285 11/19/2116:02 5 of 24 <br />