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QC Sample Results <br />Client: Calgon Carbon Corporation <br />Project/Site: Carbon Acceptance, 20200149.1 <br />Method: EPA 8260C - Volatile Organic Compounds by GC/MS (Continued) <br />Job ID: 180-101877-6 <br /> <br />Lab Sample ID: LCS 180-306063/2-A <br />Matrix: Solid <br />Analysis Batch: 306212 <br />Analyte <br />Spike <br />Added <br />LCS LCS <br />Result Qualifier <br />Client Sample ID: Lab Control Sample <br />Prep Type: Total/NA <br />Prep Batch: 306063 <br />%Rec. <br />Unit D %Rec Limits <br />Benzene 1250 1130 ug/Kg 90 76 - 116 <br />Chlorobenzene 1250 1210 ug/Kg 97 76 _ 116 <br />1,1-Dichloroethene 1250 1110 ug/Kg 89 56 - 129 <br />Toluene 1250 1110 ug/Kg 89 72 - 121 <br />Trichloroethene 1250 1160 ug/Kg 93 74 _ 119 <br />LCS LCS <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 98 64 -124 <br />Dibromofluoromethane (Surr) 109 70- 119 <br />1,2-Dichloroethane-d4 (Surr) 102 57- 127 <br />Toluene-d8 (Surr) 110 76-120 <br />Lab Sample ID: LCSD 180-306063/3-A <br />Matrix: Solid <br />Analysis Batch: 306212 <br />Client Sample ID: Lab Control Sample Dup <br />Prep Type: Total/NA <br />Prep Batch: 306063 <br />Analyte <br />Spike <br />Added <br />LCSD LCSD <br />Result Qualifier Unit D %Rec <br />%Rec. <br />Limits RPD <br />RPD <br />Limit <br />Benzene 1250 1010 ug/Kg 81 76 - 116 11 20 <br />Chlorobenzene 1250 1130 ug/Kg 90 76 _ 116 7 20 <br />1,1-Dichloroethene 1250 989 ug/Kg 79 56 _ 129 11 27 <br />Toluene 1250 1030 ug/Kg 82 72 _ 121 7 20 <br />Trichloroethene 1250 1040 ug/Kg 83 74 - 119 11 20 <br />LCSD LCSD <br />Surrogate %Recovery Qualifier Limits <br />4-Bromofluorobenzene (Surr) 90 64- 124 <br />Dibromofluoromethane (Surr) 97 70_119 <br />1,2-Dichloroethane-d4 (Surr) 90 57 _127 <br />Toluene-d8 (Surr) 100 76- 120 <br />Method: EPA 8270D - Semivolatile Organic Compounds (GC/MS) <br />Lab Sample ID: MB 180-306131/1-A <br />Matrix: Solid <br />Analysis Batch: 306266 <br />Analyte <br />MB MB <br />Result Qualifier RL Unit <br />Client Sample ID: Method Blank <br />Prep Type: Total/NA <br />Prep Batch: 306131 <br />D Prepared Analyzed Dil Fac <br />Acenaphthene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Acenaphthylene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Anthracene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Benzo[a]anthracene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Benzo[a]pyrene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Benzo[b]fluoranthene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Benzo[g,h,i]perylene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Benzo[k]fluoranthene ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Bis(2-chloroethoxy)methane ND 10000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Bis(2-chloroethyl)ether ND 2000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Bis(2-ethylhexyl) phthalate ND 20000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />4-Bromophenyl phenyl ether ND 10000 ug/Kg 02/05/20 12:25 02/06/20 13:20 1 <br />Eurofins TestAmerica, Pittsburgh <br />Page 12 of 20 2/17/2020